Éditeur(s) : HAL CCSD E Schweizerbart Science Publishers
Résumé : International audience
We present an electron tomography study of dislocations in deformed olivine single crystals, at ca. 0.5 T m, along two distinct orientations. The easiest slip systems are [001](100) and [001]{110}. Disorientating a single crystal away from easy glide conditions leads to massive cross-slip, which generates three-dimensional dislocations, and thus contributes to hardening. Fast motion of curved non-screw dislocation in those planes leaves long straight screw dislocations which bear lattice friction and control plastic strain. We have identified several hardening mechanisms. Non-screw [001] dislocations interact elastically to form dipoles. Recovery mechanisms leading to dipole annihilation are observed, but they are slow at those temperatures and produce numerous sessile loops. These loops represent obstacles for gliding dislocations. Interactions between dislocations and sessile loops produce sessile segments (super jogs), which efficiently impede dislocation motions.
ISSN: 0935-1221

hal-01277821
https://hal.archives-ouvertes.fr/hal-01277821
DOI : 10.1127/ejm/2015/0027-2481

Éditeur(s) : HAL CCSD Taylor & Francis: STM Behavioural Science and Public Health Titles Taylor & Francis: STM, Behavioural Science and Public Health Titles
Résumé : We have investigated by electron tomography, in a transmission electronic microscope, the interactions between dislocations in olivine single crystals and polycrystals deformed in axial compression at T < 1000 °C (T < 0.5Tm). Dislocations are mostly of the [0 0 1] type, except in the polycrystal where [1 0 0] and [0 0 1] dislocations have been activated. A few 〈1 0 1〉 junctions have been found and characterized. Many collinear interactions have been identified either involving direct interactions between crossing dislocations of opposite Burgers vectors or indirect interactions between dislocations gliding in parallel planes and sessile dislocation loops. We suggest that collinear interaction, already identified as the primary source of strain hardening in FCC metals, is the main dislocation interaction mechanism in olivine deformed at temperatures below 1000 °C.
ISSN: 1478-6443

hal-01174166
https://hal.archives-ouvertes.fr/hal-01174166
DOI : 10.1080/14786435.2014.1000996

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
We have performed tri-axial compression experiments on olivine aggregates at 900 °C and at a confining pressure of 300 MPa in a high-resolution gas-medium mechanical testing apparatus. Deformation at two different constant strain rates (1.1 × 10− 5 s− 1 and 3.4 × 10− 4 s− 1) yields continuous hardening, reaching maximal differential stresses of 930 and 1076 MPa, respectively, before sample failure at ca. 10% strain. The deformed samples were characterized by electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). Crystallographic preferred orientations (CPO) are weak but reveal an alignment of the [010] axes around the compression direction and some concentration of [001] and [100] axes normal to it. TEM observations confirm plastic deformation by dislocation glide, with both [001] and [100] Burgers vectors. Electron tomography, performed for the first time on deformed fined-grained olivine, shows that [001] dislocations glide extensively on {110} and {130} planes, in complement to the (010) and (100) glide planes often reported at high temperatures. [100] dislocations glide mostly on (010), but {011} and {041} planes are also activated. The experimental CPO and relative activity of slip systems are well reproduced by viscoplastic self-consistent simulations in which all [100] and [001] slip systems have similar strengths. They are also consistent with olivine CPO from natural samples deformed at low temperature. Comparison of the present mechanical results to those obtained for olivine single-crystals at similar conditions shows that at low temperature (below 1100 °C) and high stress (> 300 MPa) polycrystalline olivine has a more complex mechanical behavior than single crystals. However, both datasets advocate for a much weaker dry mantle lithosphere than previously thought.
ISSN: 0040-1951

hal-01053513
https://hal.archives-ouvertes.fr/hal-01053513
DOI : 10.1016/j.tecto.2014.03.022

Éditeur(s) : HAL CCSD Springer Verlag
Résumé : International audience
A San Carlos olivine polycrystal has been deformed under uppermost mantle conditions, by compression at 900 °C, at a strain rate of 1.1 × 10−5 s−1, under a confining pressure of 300 MPa, using the Paterson press. Transmission electron tomography of dislocations has been performed by scanning transmission electron microscopy, by conventional transmission electron microscopy using the weak-beam dark-field technique, associated with precession or not, in order to determine the glide planes of [001] screw dislocations. This recent technique is the most suitable one since most [001] dislocations exhibit straight screw segments due to the high lattice friction on this character at low temperature. We find that [001] dislocations glide in (100), (010) and {110} as already reported, but also more unexpectedly in {120} and {130}. We show that at 900 °C, [001] {110} glide is dominant in polycrystals. We have, however, noted and characterized numerous cross-slip events in the specimen.
ISSN: 0342-1791

hal-01054330
https://hal.archives-ouvertes.fr/hal-01054330
DOI : 10.1007/s00269-014-0665-1

Éditeur(s) : HAL CCSD Taylor & Francis: STM, Behavioural Science and Public Health Titles
Résumé : International audience
The dislocation microstructures in a single crystal of olivine deformed experimentally in uniaxial compression at 1090 °C and under a confining pressure of 300 MPa, have been investigated by transmission electron tomography in order to better understand deformation mechanisms at the microscale relevant for lithospheric mantle deformations. Investigation by electron tomography reveals microstructures, which are more complex than previously described, composed of and dislocations commonly exhibiting 3D configurations. Numerous mechanisms such as climb, cross-slip, double cross-slip as well as interactions like junction formations and collinear annihilations are the source of this complexity. The diversity observed advocates for microscale deformation of olivine significantly less simple than classic dislocation creep reported in metals or ice close to melting temperature. Deciphering mechanism of hardening in olivine at temperatures where ionic diffusion is slow and is then expected to play very little role is crucial to better understand and thus model deformation at larger scale and at temperatures (900–1100 °C) highly relevant for the lithospheric mantle.
ISSN: 1478-6443

hal-01667146
https://hal.archives-ouvertes.fr/hal-01667146
DOI : 10.1080/14786435.2017.1367858

Éditeur(s) : HAL CCSD IOP Publishing
Résumé : International audience
Based on the very recent work by Censor and Segal (2009 J. Convex Anal. 16 587-600) and inspired by Xu (2006 Inverse Problems 22 2021-34) and Yang (2004 Inverse Problems 20 1261-6), we investigate an algorithm for solving the split common fixed-point problem for the class of demicontractive operators in a Hilbert space. Our results improve and/or develop previously discussed feasibility problems and related algorithms. It is worth mentioning that the convex feasibility formalism is at the core of the modeling of many inverse problems and has been used to model significant real-world problems, for instance, in sensor networks, in radiation therapy treatment planning, in computerized tomography and data compression, see Censor et al (2006 Phys. Med. Biol. 51 2353-65) and Combettes (1996 Adv. Imaging Electron. Phys. 95 155-270) and references therein.
ISSN: 0266-5611

hal-00778174
https://hal.univ-antilles.fr/hal-00778174
DOI : 10.1088/0266-5611/26/5/055007

Éditeur(s) : HAL CCSD Pergamon
Résumé : This paper presents an experimental study of the deformation of Beaucaire marl subjected to drained triaxial tests under a wide range of confining pressure. Several methods of observation have been used: X-ray computed tomography, scanning electronic microscopy, quantitative image analysis of thin sections and mercury porosimetry. The analysis at the grain scale shows the existence of various deformation modes depending on the mean stress level. These modes are classified with reference to the brittle and ductile regimes. In specimens deformed under low confining pressure, macro-cracks are localised in a band more contracting than the rest of the specimen. In specimens deformed under moderate confining pressure, a series of micro-scale shear bands characterised by a grain re-orientation towards the direction of macro-shear is detected in the zones of localised deformation. The material in between the micro-scale shear bands is contracting more than the rest of the specimen in some cases; in other cases, a schistosity is detected also in the rest of the specimen outside the localisation zones. In the specimen deformed under high confining pressure, no localisation occurs, and a schistosity is observable throughout the specimen.
ISSN: 1365-1609

hal-00411208
https://hal.archives-ouvertes.fr/hal-00411208
DOI : 10.1016/j.ijrmms.2007.08.007

Éditeur(s) : HAL CCSD
Résumé : We present an experimental study of relations between hydraulic properties of clayey rocks and their deformation at bulk and micro scale. The experimentation is based on triaxial deformation of kaolinitic core samples, on permeability measurements, and on several methods of analysis of the microstructure. To produce the samples, remoulded kaolinite material is consolidated by axial loading up to 20 MPa in an oedometric cell. Then, in a triaxial cell, an undrained stress path is applied in order to induce shearing damage in the sample. The permeability of the sample is measured by fluid flow across the sample. Before and after these hydro-mechanical tests, the evolution and the homogeneity of the pore space and moreover the texture of the material are analysed by X-ray tomography, environmental scanning electron microscopy and thermic neutron diffraction. Contrary to expectations, the permeability at the sample scale does not vary significantly, although quite large deformation is reached. The final deformation is heterogeneous, with well-developed shear bands. It appears that the development of compacting and dilating zones generates a heterogeneous permeability field, which results in a negligible variation of the bulk permeability at the sample scale.
International Journal of Rock Mechanics and Mining Science

hal-00496407
https://hal.archives-ouvertes.fr/hal-00496407
DOI : 10.1016/j.ijrmms.2010.04.007