Éditeur(s) : HAL CCSD Elsevier
Résumé : We studied the evolution of the microstructure of ice-Ih during static recrystallization by stepwise annealing experiments. We alternated thermal annealing and electron backscatter diffraction (EBSD) analyses on polycrystalline columnar ice pre-deformed in uniaxial compression at temperature of −7 °C to macroscopic strains of 3.0–5.2. Annealing experiments were carried out at −5 °C and −2 °C up to a maximum of 3.25 days, typically in 5–6 steps. EBSD crystal orientation maps obtained after each annealing step permit the description of microstructural changes. Decrease in average intragranular misorientation at the sample scale and modification of the misorientation across subgrain boundaries provide evidence for recovery from the earliest stages of annealing. This initial evolution is similar for all studied samples irrespective of their initial strain or annealing temperature. After an incubation period ≥1.5 h, recovery is accompanied by recrystallization (nucleation and grain boundary migration). Grain growth proceeds at the expense of domains with high intragranular misorientations, consuming first the most misorientated parts of primary grains. Grain growth kinetics fits the parabolic growth law with grain growth exponents in the range of 2.4–4.0. Deformation-induced tilt boundaries and kink bands may slow down grain boundary migration. They are stable features during early stages of static recrystallization, only erased by normal growth, which starts after >24 h of annealing.
ISSN: 0191-8141

hal-01685644
https://hal.archives-ouvertes.fr/hal-01685644
DOI : 10.1016/j.jsg.2017.05.001

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
We investigated the deformation mechanisms and the seismic properties of 10 eclogite samples from different localities (Alps, Norway, Mali and eastern China) through the analysis of their microstructures and lattice-preferred orientations (LPO). These samples are representative of various types and intensity of deformation under eclogitic metamorphic conditions. Omphacite and garnet LPO were determined from electron backscatter diffraction (EBSD) technique. Garnet appears to be almost randomly oriented whereas omphacite develops strong LPO, characterized by the [001]-axes concentrated sub-parallel to the lineation, and the (010)-poles concentrated sub-perpendicular to the foliation. In order to analyze the deformation mechanisms that produced such omphacite LPO, we compare our observations to LPO simulated by viscoplastic self-consistent numerical models. A good fit to the measured LPO is obtained for models in which the dominant slip systems are 1/2h110i{11 ¯ 0}, [001] {110} and [001] (100). Dominant activation of these slip systems is in agreement with TEM studies of naturally deformed omphacite. Seismic properties of eclogite are calculated by combining the measured LPO and the single crystal elastic constants of omphacite and garnet. Although eclogite seismic anisotropies are very weak (less than 3% for both P-and S-wave), they are generally characterized by a maximum P-wave velocity sub-parallel to the lineation and by a minimum velocity approximately normal to foliation. The mean P-and S-wave velocities are high (respectively, 8.6 and 4.9 km/s). The S-wave anisotropy pattern displays complex relationships with the structural frame but the fast polarization plane generally tends to be parallel to the foliation. Calculated reflection coefficients show that an eclogite/crust interface is generally a good reflector (Rc > 0.1), whereas an eclogite body embedded in the upper mantle would be hardly detectable.
ISSN: 0040-1951

hal-01389715
http://hal.univ-reunion.fr/hal-01389715
http://hal.univ-reunion.fr/hal-01389715/document
http://hal.univ-reunion.fr/hal-01389715/file/Bascou_eclo-sismo_tphy2001_hal.pdf
DOI : 10.1016/S0040-1951(01)00156-1

Éditeur(s) : HAL CCSD
Résumé : Based on fieldwork and modern analytical technics, this work presents an overview of the Mid-Cretaceous hyper-extended rift system exposed in the northern part of the Pyrenean mountain range. Its inversion during the Pyrenean orogeny allows for precious observations of the deep-seated processes occurring at the foot of distal margins. Some peculiar aspects characterizing the pre-Alpine hyper-extended domain are examined throughout the 400km long suture that is fossilized in the North Pyrenean Zone (NPZ). The High Temperature/Low Pressure (HT/LP) thermal imprint of the extensional event is studied thanks to a dataset of more than hundred peak temperature measurement by Raman spectroscopy of the carbonaceous material (RSCM). The pre- and syn-rift metasediments are characterized by an intense ductile deformation. Field and EBSD investigations of the mechanisms of deformation reveal ductile and syn-metamorphic processes. The emplacement conditions of the peridotite into crustal levels and localized exhumation is examined in the key-localities of Urdach, Saraillé-Tos de la Coustette, Moncaup, Lherz, Caussou-Bestiac and Salvezines, The results indicate an early boudinage of the crust during the rifting process, resulting in the direct superposition of pre-rift sediments on top of mantle peridotites. Field, textural and isotopic characterization of the various ophicalcite and breccias found in the vicinity of the peridotite outcrops allow to decipher their exhumation history. New Ar-Ar geochronological results allow to precise the temporal evolution of the NPZ.
Cette thèse présente une analyse structurale et thermique des marges passives crétacées inversées dans la Zone Nord Pyrénéenne (ZNP). L'application du paléothermomètre RSCM (spectrométrie Raman de la matière carbonée) sur plus de cent échantillons répartis à travers la ZNP permet de préciser l'évolution thermique de la déchirure continentale. Un métamorphisme de haute température (450 à >600°C) se développe particulièrement au droit de zones ou la croûte continentale est extrêmement amincie voire éliminée. Les sédiments pré- et syn-rift sont marqués par une intense déformation ductile. L'analyse à l'EBSD des fabriques minérales indique une déformation de Haute-température contemporaine du métamorphisme HT-BP. Les conditions de mise en place crustale des péridotites et leur exhumation localisée sont examinées dans les localités d'Urdach, Saraillé-Tos de la Coustette, Moncaup, Lherz, Caussou-Bestiac et Salvezines. Les résultats indiquent un boudinage de la croûte continentale au cours du processus de rifting. Des décollements de couverture, principalement localisés dans les évaporites triasiques conduisent à la superposition directe des sédiments pré-rift sur le manteau exhumé. La notion nouvelle de soutirage crustal est introduite pour désigner ce processus dans lequel l'écoulement gravitaire ne joue pas un rôle principal. La caractérisation sédimentologique, pétrographique et isotopique (O et C) des différentes formations de brèches et ophicalcites observées à proximité des corps de péridotites permet de reconstituer les étapes de l'exhumation du manteau en pied de marge. Enfin de nouvelles datations permettent de mieux contraindre le calendrier des évènements successifs.
https://tel.archives-ouvertes.fr/tel-00787952

tel-00787952
https://tel.archives-ouvertes.fr/tel-00787952
https://tel.archives-ouvertes.fr/tel-00787952/document
https://tel.archives-ouvertes.fr/tel-00787952/file/TheI_se-Clerc-2012.pdf

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
The nucleation and growth processes of spherulitic alkali feldspar have been investigated in this study through X-ray microtomography and electron backscatter diffraction (EBSD) data. Here we present the first data on Shape Preferred Orientation (SPO) and Crystal Preferred Orientation (CPO) of alkali feldspar within spherulites. The analysis of synchrotron X-ray microtomography and EBSD datasets allowed us to study the morphometric characteristics of spherulites in trachytic melts in quantitative fashion, highlighting the three-dimensional shape, preferred orientation, branching of lamellae and crystal twinning, providing insights about the nucleation mechanism involved in the crystallization of the spherulites. The nucleation starts with a heterogeneous nucleus (pre-existing crystal or bubble) and subsequently it evolves forming “bow tie” morphologies, reaching radially spherulitic shapes in few hours. Since each lamella within spherulite is also twinned, these synthetic spherulites cannot be considered as single nuclei but crystal aggregates originated by heterogeneous nucleation. A twin boundary may have a lower energy than general crystal–crystal boundaries and many of the twinned grains show evidence of strong local bending which, combined with twin plane, creates local sites for heterogeneous nucleation.This study shows that the growth rates of the lamellae (10− 6–10− 7 cm/s) in spherulites are either similar or slightly higher than that for single crystals by up to one order of magnitude. Furthermore, the highest volumetric growth rates (10− 11–10− 12 cm3/s) show that the alkali feldspar within spherulites can grow fast reaching a volumetric size of ~ 10 μm3 in 1 s.
ISSN: 0024-4937

hal-01172356
https://hal.archives-ouvertes.fr/hal-01172356
DOI : 10.1016/j.lithos.2014.12.003

Éditeur(s) : HAL CCSD Wiley-Blackwell
Résumé : International audience
Garnet growth in high-pressure, mafic garnet granulites formed by dehydration melting of hornblende-gabbronorite protoliths in the Jijal complex (Kohistan palaeo-island arc complex, north Pakistan) was investigated through a microstructural EBSD-SEM and HRTEM study. Composite samples preserve a sharp transition in which the low-pressure precursor is replaced by garnet through a millimetre-sized reaction front. A magmatic foliation in the gabbronorite is defined by mafic-rich layering, with an associated magmatic lineation defined by the shape-preferred orientation (SPO) of mafic clusters composed of orthopyroxene (Opx), clinopyroxene (Cpx), amphibole (Amp) and oxides. The shape of the reaction front is convoluted and oblique to the magmatic layering. Opx, Amp and, to a lesser extent, Cpx show a strong lattice-preferred orientation (LPO) characterized by an alignment of [001] axes parallel to the magmatic lineation in the precursor hornblende-gabbronorite. Product garnet (Grt) also displays a strong LPO. Two of the four < 111 > axes are within the magmatic foliation plane and the density maximum is subparallel to the precursor magmatic lineation. The crystallographic relationship < 111 >(Grt)//[001](Opx,Cpx,Amp) deduced from the LPO was confirmed by TEM observations. The sharp and discontinuous modal and compositional variations observed at the reaction front attest to the kinetic inhibition of prograde solid-state reactions predicted by equilibrium-phase diagrams. The P-T field for the equilibration of Jijal garnet granulites shows that the reaction affinities are 5-10 kJ mol.(-1) for the Grt-in reaction and 0-5 kJ mol.(-1) for the Opx-out reaction. Petrographic and textural observations indicate that garnet first nucleated on amphibole at the rims of mafic clusters; this topotactic replacement resulted in a strong LPO of garnet. Once the amphibole was consumed in the reaction, the parallelism of [001] axes of the mafic-phase reactants favoured the growth of garnet crystals with similar orientations over a pyroxene substrate. These aggregates eventually sintered into single-crystal garnet. In the absence of deformation, the orientation of mafic precursor phases conditioned the nucleation site and the crystallographic orientation of garnet because of topotaxial transformation reactions and homoepitaxial growth of garnet during the formation of high-pressure, mafic garnet-granulite after low-pressure mafic protoliths.
ISSN: 0263-4929

hal-00411323
https://hal.archives-ouvertes.fr/hal-00411323
DOI : 10.1111/J.1525-1314.2008.00789.x

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
We have performed tri-axial compression experiments on olivine aggregates at 900 °C and at a confining pressure of 300 MPa in a high-resolution gas-medium mechanical testing apparatus. Deformation at two different constant strain rates (1.1 × 10− 5 s− 1 and 3.4 × 10− 4 s− 1) yields continuous hardening, reaching maximal differential stresses of 930 and 1076 MPa, respectively, before sample failure at ca. 10% strain. The deformed samples were characterized by electron backscatter diffraction (EBSD) and transmission electron microscopy (TEM). Crystallographic preferred orientations (CPO) are weak but reveal an alignment of the [010] axes around the compression direction and some concentration of [001] and [100] axes normal to it. TEM observations confirm plastic deformation by dislocation glide, with both [001] and [100] Burgers vectors. Electron tomography, performed for the first time on deformed fined-grained olivine, shows that [001] dislocations glide extensively on {110} and {130} planes, in complement to the (010) and (100) glide planes often reported at high temperatures. [100] dislocations glide mostly on (010), but {011} and {041} planes are also activated. The experimental CPO and relative activity of slip systems are well reproduced by viscoplastic self-consistent simulations in which all [100] and [001] slip systems have similar strengths. They are also consistent with olivine CPO from natural samples deformed at low temperature. Comparison of the present mechanical results to those obtained for olivine single-crystals at similar conditions shows that at low temperature (below 1100 °C) and high stress (> 300 MPa) polycrystalline olivine has a more complex mechanical behavior than single crystals. However, both datasets advocate for a much weaker dry mantle lithosphere than previously thought.
ISSN: 0040-1951

hal-01053513
https://hal.archives-ouvertes.fr/hal-01053513
DOI : 10.1016/j.tecto.2014.03.022

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
The Espinho Branco anatexite, located within a transcurrent, high-temperature shear zone in NE Brazil, was the subject of a comprehensive petrostructural study (Anisotropy of Magnetic Susceptibility - AMS, Anisotropy of Anhysteretic Remanence - AAR, Electron Backscatter Diffraction - EBSD) to evaluate the compatibility of different fabrics with the kinematics of melt deformation. Magnetite dominates susceptibilities larger than 1 mSI and biotite displays [001] lattice directions consistent with AMS k3 axes. In contrast, migmatites with a susceptibility lower than 0.5 mSI and no visible mesoscopic foliation provide crystallographic fabrics distinct from AMS and AAR. However, AAR remains consistent with the regional strain field. These results suggest that the correlation of field, AMS and crystallographic fabrics is not always straightforward despite the relatively simple organisation of the magnetic fabric in the anatexite. We conclude that AMS recorded the final stages of the strain field in the migmatite irrespective of its complex mesoscale structures and contrasting crystallographic fabrics.
ISSN: 0191-8141

hal-00823056
https://hal.archives-ouvertes.fr/hal-00823056
DOI : 10.1016/j.jsg.2012.12.008

Éditeur(s) : HAL CCSD
Résumé : This thesis compiles two distinct studies that both document the control of microstructures on rock seismic properties. The first part deals with the development of crystallographic preferred orientations (CPO) in the uppermost mantle associated with melt/fluid-rock interactions, recorded in peridotites xenoliths from the Japan sea back-arc basin. The microstructural and geochemical characteristics of the studied samples reveal that active spreading is associated to uppermost mantle deformation similar to that observed in the Oman ophiolite. At the onset of back-arc spreading, there are no strong interactions between melt percolation and deformation in comparison to continental rift zones, probably due to the relatively small size and short duration of the spreading event. The second part presents a unique database of plagioclase CPO from variously deformed mafic rocks. CPO are grouped in three main types; their characteristics as a function of deformation regime (magmatic or crystal-plastic) are outlined and discussed. Calculated seismic properties of gabbroic rocks show that anisotropy tends to increase as a function of fabric strength, although it is generally weak, due to the competing effect of olivine/clinopyroxene and plagioclase.
Cette thèse regroupe deux études distinctes, qui documentent le contrôle des microstructures sur les propriétés sismiques des roches. La première partie traite du développement des orientations préférentielles cristallographiques (OPC) dans le manteau supérieur, associé aux interactions liquide/magma-roche, enregistré dans des xénolites de péridotites du bassin d'arrière-arc de la mer du Japon. Les caractéristiques microstucturales et géochimiques des échantillons étudiés montrent que l'ouverture arrière-arc active est associée à une déformation du manteau supérieure similaire à celle observée dans l'ophiolite d'Oman. L'initiation de l'extension d'arrière-arc n'est pas associée à de fortes interactions entre percolation magmatique et déformation, en comparaison avec les zones de rifting continentales, probablement en raison des taille et durée relativement petites de l'épisode d'ouverture. La seconde partie présente une base de données unique d'OPC de plagioclase de roches mafiques plus ou moins déformées. Les OPC sont classées en 3 types principaux; leurs caractéristiques en fonction du régime de déformation (magmatique ou plastique) sont présentées et discutées. Les propriétés sismiques calculées des roches gabbroiques montrent que l'anisotropie tend à croitre avec l'intensité des fabriques, bien qu'elle soit généralement faible, en raison des effets opposés des olivines/clinopyroxènes et du plagioclase.
https://tel.archives-ouvertes.fr/tel-00795505

tel-00795505
https://tel.archives-ouvertes.fr/tel-00795505
https://tel.archives-ouvertes.fr/tel-00795505/document
https://tel.archives-ouvertes.fr/tel-00795505/file/Satsukawa_thesis_UM2.pdf

Éditeur(s) : HAL CCSD Elsevier
Résumé : Folds with hinge lines subparallel to stretching lineation are common features in shear zones and represent extreme cases of fold modification. However, their microstructures and in particular their kinematic significance remain poorly understood. Here we describe the meso- and micro-scale structures and crystallographic preferred orientation (CPO) of quartz and muscovite from a metric-scale shear-modified fold from Plattjen, Saas Fee, Western Internal Alps. The studied fold is of class-2 and the samples collected around the fold have essentially the same microstructures. Quartz [c]-axes plotted in the tectonic coordinate system exhibit an apparent reverse obliquity on opposing limbs. Muscovite fabrics are controlled essentially by the orientation of {001} planes. If the CPO data are plotted in a common reference frame (e.g. either fold or geographical), all samples exhibit essentially the same patterns for both minerals. In particular, relative to the fold axis and axial surface, the reversal of quartz CPO obliquity on opposing limbs is no longer evident. The small obliquity (~ 15°) between the intersection lineation of the two planes of {001} of muscovite and the fold axis results in the apparent reversal of shear sense on opposite limbs when viewing the CPO related to the macroscopic fabric. The homogeneity of the microstructures and CPOs of quartz and muscovite across the fold support the interpretation that the fold developed during simultaneous activation of heterogeneous and homogeneous simple shear, with the former responsible for fold development and the latter responsible for fold rotation and the overwhelming of the heterogeneous deformation. These processes led to the observed parallelism between fold hinge line and local stretching lineation.
ISSN: 0040-1951

hal-00824537
https://hal.archives-ouvertes.fr/hal-00824537
DOI : 10.1016/j.tecto.2011.03.003

Éditeur(s) : HAL CCSD Mineralogical Society of America
Résumé : International audience
In situ mineralization of CO2 in ultramafic rock-hosted aquifers is one of the promising solutions for decreasing CO2 concentrations in the atmosphere. Naturally altered ultramafic rocks suggest that carbonation processes are controlled by local heterogeneities in the structure of the rock and fluid transport at the water-rock interfaces. We studied the role of rock crystallographic anisotropy relative to the global fluid flow direction on the mineralization of CO2 by means of electron microscope analyses from the macro- to the micrometer scale (EBSD-FIB). The sample used for the measurements was a hot pressed olivine core percolated by water enriched in CO2 (pCO2 = 10 MPa) at 180 °C. During the percolation experiment, olivine was dissolved and two types of carbonates, dolomite, and magnesite, were precipitated on olivine surfaces. The results showed that the dissolution of olivine is controlled by its crystallographic properties as shown by the development of etch-pits only on the (010)ol planes and with elongated shapes parallel to the [010]ol axes. In contrast, the precipitation of carbonates is governed by hydrodynamic properties. Carbonates are heterogeneously distributed in the percolated rock. They are mainly located along the moderate (for dolomite) and the minor (for magnesite) flow paths, both oriented parallel to the principal fluid flow direction, which allow carbonates to be supplied with divalent cations (e.g., Ca2+, Mg2+, and Fe2+). In these flow paths, carbonate growth is systematically oriented normal to the flow that facilitates the development of chemical gradients with cationic supersaturation conditions for carbonate precipitation near the walls.In natural systems, the (010)ol planes are parallel to the Moho and the (100)ol planes are vertical; our study suggests that flow of CO2-rich fluids will induce precipitation of carbonates localized along, and preferentially clogging, vertical flow paths while favoring olivine dissolution along horizontal fluid pathways. This dual control of structure and fluid flow on carbonation mechanisms could be an important parameter allowing sustainable CO2 storage in peridotites, while limiting the risks of leakage toward the surface.
ISSN: 0003-004X

hal-01143393
https://hal.archives-ouvertes.fr/hal-01143393
DOI : 10.2138/am-2015-4913

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
We report gabbroic dikes in the plagioclase tectonite domains of the Ojén and Ronda massifs (Betic Cordillera, southern Spain), which record crystallization at low-pressure syn-, or slightly postkinematic to the late ductile history of the Betic Peridotite in the westernmost Mediterranean. We present mineral major and trace element compositional data of discordant gabbroic dikes in the Ojén massif and gabbroic patches in the Ronda massif, complemented by the whole rock and electron backscattered diffraction (EBSD) data of the Ojén occurrence. In the Ojén massif, gabbro occurs as 1–3 centimeter wide discordant dikes that crosscut the plagioclase tectonite foliation at high angle. These dikes are composed of cm-scale igneous plagioclase and clinopyroxene crystals that show shape preferred orientations subparallel to the lineation of the host peridotite and oblique to the trend of the dike. Intrusion of Ojén gabbro dikes is coherent with the stress field that formed the high temperature, ductile plagioclase tectonite foliation and then attests for a mantle igneous event prior to the intracrustal emplacement of the massif. In the Ronda massif, gabbroic rocks crystallized in subcentimeter wide anastomozing veins, or as interstitial patches in the host dunite. They are mostly composed of plagioclase and clinopyroxene. Plagioclase composition is bytownitic in the Ojén, and andesinic in the Ronda massif. Clinopyroxene in both places shows identical, light Rare-Earth Element (LREE) depleted trace element patterns. The calculated trace element composition of melts in exchange equilibrium with the studied igneous clinopyroxenes reflects LREE-enriched character coupled with negative Eu anomaly, and indicates that gabbro-forming melts in Ronda and Ojén share a common melt source with an island arc tholeiitic affinity. Geothermobarometric data and liquidus mineralogy indicate that gabbro crystallization occurred at shallow depths (0.2–0.5 GPa) in a 7–16 km thick lithospheric section. These data suggest that gabbro-forming melts in the Betic Peridotite record a mantle igneous event at very shallow depths and provide evidence for the hyperextension of the continental lithosphere compatible with extreme backarc basin extension induced by the slab rollback of the Cenozoic subduction system in the westernmost Mediterranean.
ISSN: 0040-1951

hal-01172246
https://hal.archives-ouvertes.fr/hal-01172246
DOI : 10.1016/j.tecto.2015.03.011

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
We have inferred the deformation mechanisms of antigorite by high-resolution EBSD mapping of samples from Cerro del Almirez ultramafic massif (Betic Cordillera, SE Spain). Textural relations and phase diagram calculations constrain the foliation development conditions to the subduction prograde path at up to 600-630 °C and 1.6-1.9 GPa. Deformation was followed by static annealing of antigorite at ca. 680 °C. The Crystal Preferred Orientation (CPO) of antigorite is characterised by a strong alignment of (001) poles normal to the foliation plane and a weaker, but clear, parallelism between [100] axes and the macroscopic lineation defined by the elongation of magnetite aggregates. Analysis of misorientations across subgrains shows predominance of [010] rotation axis, consistent with activation of the [100](001) slip system. However, tilt subgrain boundaries subparallel to (100), probably formed by edge dislocations of this system, are subsidiary. Most subgrain boundaries are subparallel to (001) planes. They are interpreted as (001) twins wherein continuing viscoplastic deformation resulted in a slight increase of the misorientation between the twins. Modelling of the evolution of the antigorite CPO using a lower bound approach and considering different deformation regimes and sets of basal and non-basal slip systems has shown that intensities of [100] and [010] maxima reflect the relative strength of the antigorite [100](001) and [010](001) systems. Activation of other basal or non-basal slip systems does not change significantly the CPO patterns, but results in less concentrated CPO. 3D transpression models better reproduce the CPO of natural antigorite serpentinites. We propose that the widespread occurrence of strong CPO in high-pressure antigorite serpentinite is consistent with deformation by dislocation creep with dominant glide on [hk0](001), together with the activation of twinning, implying that a power law rheology would better account for the mechanical behaviour of antigorite serpentinite deep in the subduction channel and mantle wedge.
ISSN: 0012-821X

hal-00795511
https://hal.archives-ouvertes.fr/hal-00795511
DOI : 10.1016/j.epsl.2012.06.049

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
This paper presents Digital Image Correlation (DIC) and Infrared Thermography (IRT) methods to investigate the thermomechanical behavior of an aluminum at the microstructural scale. Electron BackScattered Diffraction (EBSD) is used to characterize the microstructure of a 3 mm thick specimen with centimetric grain size. This study combines the following imaging techniques: DIC to obtain displacement and strain fields during the test, and IRT to estimate temperature and heat source fields induced by the mechanical loading. Ultimately, the aim of this methodology is to provide energy balance during mechanical test at the scale of the microstructure, in order to propose thermomechanical con-stitutive modelling of crystalline plasticity.
ISSN: 0143-8166

hal-01287711
https://hal.archives-ouvertes.fr/hal-01287711
https://hal.archives-ouvertes.fr/hal-01287711/document
https://hal.archives-ouvertes.fr/hal-01287711/file/Local_experimental_investigations_Li_al_2016.pdf
DOI : 10.1016/j.optlaseng.2016.01.001

Éditeur(s) : HAL CCSD Frontiers Media
Résumé : International audience
We present high resolution observations of microstructure and texture evolution during dynamic recrystallization (DRX) of ice polycrystals deformed in the laboratory at high temperature (≈0.98Tm). Ice possesses a significant viscoplastic anisotropy that induces strong strain heterogeneities, which result in an early occurrence of DRX mechanisms. It is therefore a model material to explore these mechanisms. High resolution c-axis measurements at sample scale by optical techniques and full crystallographic orientation measurements by cryo-Electron Back Scattering Diffraction (EBSD) provide a solid database for analyzing the relative impact of the macroscopic imposed stress vs. the local and internal stress fields on DRX mechanisms. Analysis of misorientation gradients in the EBSD data highlights a heterogeneous dislocation distribution, which is quantified by the Nye tensor estimation. Joint analyses of the dislocation density maps and microstructural observations highlight spatial correlation between high dislocation density sites and the onset of nucleation taking place by grain-boundary bulging, subgrain rotation or by the formation of kink-bands.
ISSN: 2296-6463

hal-01515284
https://hal.univ-lorraine.fr/hal-01515284
DOI : 10.3389/feart.2015.00081

Éditeur(s) : HAL CCSD
Résumé : National audience
Les semelles métamorphiques sont situées à la base desgrandes ophiolites obductées. Elles sont principalement composéesd’amphibolites (métabasaltes à amphiboles ± grenat,clinopyroxène, plagioclase) fortement cisaillées et dont les conditionsmaximum de métamorphisme sont estimées à 800±100Cet 1.0±0.2 GPa. Leur formation a lieu au cours des 2 Ma suivantl’initiation des zones de subduction. Ces amphibolites sont interprétéescomme des portions de lithosphère océanique subduite,portions qui sont métamorphisées, dis-je, à haute températurepar transfert de chaleur depuis le coin de manteau sus-jacent quiformera la base de l’ophiolite obductée. Leur importante déformationau pic de métamorphisme est interprétée comme synchroneà leur accrétion au manteau de la plaque supérieure. Les semellesmétamorphiques sont donc des témoins directs de la dynamiqueprécoce des zones de subduction océanique. Leur pétrologie etleur déformation fournissent des contraintes majeures, et rares,sur l’évolution de la structure thermique et sur le comportementmécanique de l‘interface de subduction naissante. Cette étudeprésente des données structurales à plusieurs échelles, couplant desanalyses de terrain aux analyses EBSD sur des échantillons à amphibole± plagioclase ± clinopyroxene ± grenat de la semelle métamorphique.Les grains d’amphibole et de plagioclase sont caractériséspar une forte orientation préférentielle parallèle à la foliationet à la linéation. Cette fabrique est accompagnée par une forteorientation cristallographique préférentielle des amphiboles marquéepar un axe [001] marquant la linéation et la normale au plan(001) perpendiculaire à la foliation. Les plagioclases montrentune orientation cristallographique préférentielle faible voire nulle.Cette fabrique est similaire à celle observée dans les amphibolitescisaillées de base de croûte continentale. Les clinopyroxèneset les grenats présentent des degrés d’orientation intermédiaires.Ces deux phases forment des boudins dont l’axe long est orientéparallèlement à la foliation. Les porphyroclastes de clinopyroxèneprésentent une extinction ondulante et le développement de sousgrainsà leur périphérie. Les clinopyroxènes et les grenats agissentdonc comme phases ” dures ”, augmentant la résistance de laroche à la déformation. À l’initiation de la subduction, la partiesupérieure de la plaque plongeante est affectée par l’augmentationprogressive du degré de métamorphisme. Ceci entraîne une fortedéshydratation et la cristallisation de phases ” faibles ” (quartz,amphibole, plagioclase) et ” fortes ” (clinopyroxene, grenat). Larhéologie de l’interface de la subduction en est fortement affectée.Les unités de la semelle métamorphique (avec des minéralogies etdes conditions P-T-t différentes) accrétées aux péridotites de laplaque supérieure témoignent de changements rhéologiques majeuresà l’interface de la subduction au cours de l’histoire précocedes zones de subduction.
RST 2016, livre des résumés
Caen, France

insu-01388730
https://hal-insu.archives-ouvertes.fr/insu-01388730

Éditeur(s) : HAL CCSD Springer
Résumé : International audience
Thermoelastic behavior of different marble types was analyzed using computational modeling and experimental measurements. Eight marble samples with different composition, grain size, grain boundary geometry, and texture were investigated. Calcitic and dolomitic marbles were considered. The average grain size varies from 75 μm to 1.75 mm; grain boundary geometry differs from nearly equigranular straight grain boundaries to inequigranular-interlobate grain boundaries. Four typical marble texture types were observed by EBSD measurements: weak texture; strong texture; girdle texture and high-temperature texture. These crystallographic orientations were used in conjunction with microstructure-based finite element analysis to compute the thermoelastic responses of marble upon heating. Microstructural response maps highlight regions and conditions in the marble fabric that are susceptible to degradation phenomena. This behavior was compared to the measured thermal expansion behavior, which shows increasing residual strains upon repetitive heating-cooling cycles. The thermal expansion behavior as a function of temperature changes can be classified into four categories: (a) isotropic thermal expansion with small or no residual strain; (b) anisotropic thermal expansion with small or no residual strain; (c) isotropic thermal expansion with a residual strain; and (d) anisotropic thermal expansion with residual strain. Thermal expansion coefficients were calculated for both simulated and experimental data and also modeled from the texture using the MTEX software. Fabric parameters control the amount and directional dependence of the thermal expansion. Marbles with strong texture show higher directional dependence of the thermal expansion coefficients and have smaller microstructural values of the maximum principal stress and strain energy density, the main precursors of microcracking throughout the marble fabric. In contrast, marbles with weak texture show isotropic thermal expansion behavior, have a higher propensity to microcracking, and exhibit higher values of maximum principal stress and strain energy density. Good agreement between the experimental and computational results is observed, demonstrating that microstructure-based finite-element simulations are an excellent tool for elucidating influences of rock fabric on thermoelastic behavior.
ISSN: 1866-6280

hal-00858095
https://hal.archives-ouvertes.fr/hal-00858095
DOI : 10.1007/s12665-013-2406-z

Éditeur(s) : HAL CCSD Geological Society of London
Résumé : This paper presents the background for the calculation of physical properties of an aggregate from constituent crystal properties and the texture of the aggregate in a coherent manner. Emphasis is placed on the important tensor properties of 2nd and 4th rank with applications in rock deformation, structural geology, geodynamics and geophysics. We cover texture information that comes from pole figure diffraction and single orientation measurements (electron backscattered diffraction or EBSD, electron channelling pattern, Laue pattern, optical microscope universal-stage). In particular, we provide explicit formulae for the calculation of the averaged tensor from individual orientations or from an orientation distribution function (ODF). For the latter we consider numerical integration and an approach based on the expansion into spherical harmonics. This paper also serves as a reference paper for the mathematical tensor capabilities of the texture analysis software MTEX, which is a comprehensive, freely available MatLab toolbox that covers a wide range of problems in quantitative texture analysis, for example, ODF modelling, pole figure to ODF inversion, EBSD data analysis and grain detection. MTEX offers a programming interface which allows the processing of involved research problems as well as highly customizable visualization capabilities; MTEX is therefore ideal for presentations, publications and teaching demonstrations.
Deformation Mechanisms, Rheology and Tectonics: Microstructures, Mechanics and Anisotropy

hal-00688833
https://hal.archives-ouvertes.fr/hal-00688833

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
Prediction of ice mass flow and associated dynamics is pivotal at a time of climate change. Ice flow is dominantly accommodated by the motion of crystal defects – the dislocations. In the specific case of ice, their observation is not always accessible by means of the classical tools such as X-ray diffraction or transmission electron microscopy (TEM). Part of the dislocation population, the geometrically necessary dislocations (GNDs) can nevertheless be constrained using crystal orientation measurements via electron backscattering diffraction (EBSD) associated with appropriate analyses based on the Nye (1950) approach. The present study uses the Weighted Burgers Vectors, a reduced formulation of the Nye theory that enables the characterization of GNDs. Applied to ice, this method documents, for the first time, the presence of dislocations with non-basal or Burgers vectors. These or dislocations represent up to of the GNDs observed in laboratory-deformed ice samples. Our findings offer a more complex and comprehensive picture of the key plasticity processes responsible for polycrystalline ice creep and provide better constraints on the constitutive mechanical laws implemented in ice sheet flow models used to predict the response of Earth ice masses to climate change.
ISSN: 0012-821X

hal-01685565
https://hal.archives-ouvertes.fr/hal-01685565
DOI : 10.1016/j.epsl.2017.06.020

Éditeur(s) : HAL CCSD American Geophysical Union (AGU)
Résumé : Mantle xenoliths in Pliocene alkali basalts of the eastern Betics (SE Iberia, Spain) are spinel ± plagioclase lherzolite, with minor harzburgite and wehrlite, displaying porphyroclastic or equigranular textures. Equigranular peridotites have olivine crystal preferred orientation (CPO) patterns similar to those of porphyroclastic xenoliths but slightly more dispersed. Olivine CPO shows [100]-fiber patterns characterized by strong alignment of [100]-axes subparallel to the stretching lineation and a girdle distribution of [010]-axes normal to it. This pattern is consistent with simple shear or transtensional deformation accommodated by dislocation creep. One xenolith provides evidence for synkinematic reactive percolation of subduction-related Si-rich melts/fluids that resulted in oriented crystallization of orthopyroxene. Despite a seemingly undeformed microstructure, the CPO in orthopyroxenite veins in composite xenoliths is identical to those of pyroxenes in the host peridotite, suggesting late-kinematic crystallization. Based on these observations, we propose that the annealing producing the equigranular microstructures was triggered by melt percolation in the shallow subcontinental lithospheric mantle coeval to the late Neogene formation of veins in composite xenoliths. Calculated seismic properties are characterized by fast propagation of P waves and polarization of fast S waves parallel to olivine [100]-axis (stretching lineation). These data are compatible with present-day seismic anisotropy observations in SE Iberia if the foliations in the lithospheric mantle are steeply dipping and lineations are subhorizontal with ENE strike, implying dominantly horizontal mantle flow in the ENE-WSW direction within vertical planes, that is, subparallel to the paleo-Iberian margin. The measured anisotropy could thus reflect a lithospheric fabric due to strike-slip deformation in the late Miocene in the context of WSW tearing of the subducted south Iberian margin lithosphere.
ISSN: 0278-7407

Droits : info:eu-repo/semantics/OpenAccess
hal-01685809
https://hal.archives-ouvertes.fr/hal-01685809
https://hal.archives-ouvertes.fr/hal-01685809/document
https://hal.archives-ouvertes.fr/hal-01685809/file/Hidas_et_al-2016-Tectonics.pdf
DOI : 10.1002/2016TC004165

Éditeur(s) : HAL CCSD Trans Tech Publications Inc.
Résumé : Two, high purity, Al-0.1 and 0.3wt%Mn alloys have been cold deformed in plane strain compression to strains of order 1.8 and the kinetics of subsequent recovery by sub-grain coarsening during annealing at 150-300°C measured by high resolution FEG-SEM EBSD. Accurate sub-grain size and misorientation distributions and their evolution with time and temperature have been determined. The average growth rates are then used to estimate the sub-grain boundary mobilities. Growth is analyzed by two well-known growth laws for the average sub-grain size δ (t): i) the standard relation for grain growth: where the exponent n takes values of 2-8 and ii) the relation proposed by Nes for dislocation climb in sub-grain walls: It is shown that the latter relation gives a better fit with the data in terms of the time and temperature dependence of the sub-grain sizes. In particular the activation energies for the logarithmic law are much closer to the values expected for solute-controlled movement of sub-boundaries.
Materials Science Forum

hal-00795441
https://hal.archives-ouvertes.fr/hal-00795441
DOI : 10.4028/www.scientific.net/MSF.715-716.725