Éditeur(s) : HAL CCSD Elsevier
Résumé : We studied the evolution of the microstructure of ice-Ih during static recrystallization by stepwise annealing experiments. We alternated thermal annealing and electron backscatter diffraction (EBSD) analyses on polycrystalline columnar ice pre-deformed in uniaxial compression at temperature of −7 °C to macroscopic strains of 3.0–5.2. Annealing experiments were carried out at −5 °C and −2 °C up to a maximum of 3.25 days, typically in 5–6 steps. EBSD crystal orientation maps obtained after each annealing step permit the description of microstructural changes. Decrease in average intragranular misorientation at the sample scale and modification of the misorientation across subgrain boundaries provide evidence for recovery from the earliest stages of annealing. This initial evolution is similar for all studied samples irrespective of their initial strain or annealing temperature. After an incubation period ≥1.5 h, recovery is accompanied by recrystallization (nucleation and grain boundary migration). Grain growth proceeds at the expense of domains with high intragranular misorientations, consuming first the most misorientated parts of primary grains. Grain growth kinetics fits the parabolic growth law with grain growth exponents in the range of 2.4–4.0. Deformation-induced tilt boundaries and kink bands may slow down grain boundary migration. They are stable features during early stages of static recrystallization, only erased by normal growth, which starts after >24 h of annealing.
ISSN: 0191-8141

hal-01685644
https://hal.archives-ouvertes.fr/hal-01685644
DOI : 10.1016/j.jsg.2017.05.001

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
We investigated the deformation mechanisms and the seismic properties of 10 eclogite samples from different localities (Alps, Norway, Mali and eastern China) through the analysis of their microstructures and lattice-preferred orientations (LPO). These samples are representative of various types and intensity of deformation under eclogitic metamorphic conditions. Omphacite and garnet LPO were determined from electron backscatter diffraction (EBSD) technique. Garnet appears to be almost randomly oriented whereas omphacite develops strong LPO, characterized by the [001]-axes concentrated sub-parallel to the lineation, and the (010)-poles concentrated sub-perpendicular to the foliation. In order to analyze the deformation mechanisms that produced such omphacite LPO, we compare our observations to LPO simulated by viscoplastic self-consistent numerical models. A good fit to the measured LPO is obtained for models in which the dominant slip systems are 1/2h110i{11 ¯ 0}, [001] {110} and [001] (100). Dominant activation of these slip systems is in agreement with TEM studies of naturally deformed omphacite. Seismic properties of eclogite are calculated by combining the measured LPO and the single crystal elastic constants of omphacite and garnet. Although eclogite seismic anisotropies are very weak (less than 3% for both P-and S-wave), they are generally characterized by a maximum P-wave velocity sub-parallel to the lineation and by a minimum velocity approximately normal to foliation. The mean P-and S-wave velocities are high (respectively, 8.6 and 4.9 km/s). The S-wave anisotropy pattern displays complex relationships with the structural frame but the fast polarization plane generally tends to be parallel to the foliation. Calculated reflection coefficients show that an eclogite/crust interface is generally a good reflector (Rc > 0.1), whereas an eclogite body embedded in the upper mantle would be hardly detectable.
ISSN: 0040-1951

hal-01389715
http://hal.univ-reunion.fr/hal-01389715
http://hal.univ-reunion.fr/hal-01389715/document
http://hal.univ-reunion.fr/hal-01389715/file/Bascou_eclo-sismo_tphy2001_hal.pdf
DOI : 10.1016/S0040-1951(01)00156-1

Éditeur(s) : HAL CCSD
Résumé : Based on fieldwork and modern analytical technics, this work presents an overview of the Mid-Cretaceous hyper-extended rift system exposed in the northern part of the Pyrenean mountain range. Its inversion during the Pyrenean orogeny allows for precious observations of the deep-seated processes occurring at the foot of distal margins. Some peculiar aspects characterizing the pre-Alpine hyper-extended domain are examined throughout the 400km long suture that is fossilized in the North Pyrenean Zone (NPZ). The High Temperature/Low Pressure (HT/LP) thermal imprint of the extensional event is studied thanks to a dataset of more than hundred peak temperature measurement by Raman spectroscopy of the carbonaceous material (RSCM). The pre- and syn-rift metasediments are characterized by an intense ductile deformation. Field and EBSD investigations of the mechanisms of deformation reveal ductile and syn-metamorphic processes. The emplacement conditions of the peridotite into crustal levels and localized exhumation is examined in the key-localities of Urdach, Saraillé-Tos de la Coustette, Moncaup, Lherz, Caussou-Bestiac and Salvezines, The results indicate an early boudinage of the crust during the rifting process, resulting in the direct superposition of pre-rift sediments on top of mantle peridotites. Field, textural and isotopic characterization of the various ophicalcite and breccias found in the vicinity of the peridotite outcrops allow to decipher their exhumation history. New Ar-Ar geochronological results allow to precise the temporal evolution of the NPZ.
Cette thèse présente une analyse structurale et thermique des marges passives crétacées inversées dans la Zone Nord Pyrénéenne (ZNP). L'application du paléothermomètre RSCM (spectrométrie Raman de la matière carbonée) sur plus de cent échantillons répartis à travers la ZNP permet de préciser l'évolution thermique de la déchirure continentale. Un métamorphisme de haute température (450 à >600°C) se développe particulièrement au droit de zones ou la croûte continentale est extrêmement amincie voire éliminée. Les sédiments pré- et syn-rift sont marqués par une intense déformation ductile. L'analyse à l'EBSD des fabriques minérales indique une déformation de Haute-température contemporaine du métamorphisme HT-BP. Les conditions de mise en place crustale des péridotites et leur exhumation localisée sont examinées dans les localités d'Urdach, Saraillé-Tos de la Coustette, Moncaup, Lherz, Caussou-Bestiac et Salvezines. Les résultats indiquent un boudinage de la croûte continentale au cours du processus de rifting. Des décollements de couverture, principalement localisés dans les évaporites triasiques conduisent à la superposition directe des sédiments pré-rift sur le manteau exhumé. La notion nouvelle de soutirage crustal est introduite pour désigner ce processus dans lequel l'écoulement gravitaire ne joue pas un rôle principal. La caractérisation sédimentologique, pétrographique et isotopique (O et C) des différentes formations de brèches et ophicalcites observées à proximité des corps de péridotites permet de reconstituer les étapes de l'exhumation du manteau en pied de marge. Enfin de nouvelles datations permettent de mieux contraindre le calendrier des évènements successifs.
https://tel.archives-ouvertes.fr/tel-00787952

tel-00787952
https://tel.archives-ouvertes.fr/tel-00787952
https://tel.archives-ouvertes.fr/tel-00787952/document
https://tel.archives-ouvertes.fr/tel-00787952/file/TheI_se-Clerc-2012.pdf

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
The nucleation and growth processes of spherulitic alkali feldspar have been investigated in this study through X-ray microtomography and electron backscatter diffraction (EBSD) data. Here we present the first data on Shape Preferred Orientation (SPO) and Crystal Preferred Orientation (CPO) of alkali feldspar within spherulites. The analysis of synchrotron X-ray microtomography and EBSD datasets allowed us to study the morphometric characteristics of spherulites in trachytic melts in quantitative fashion, highlighting the three-dimensional shape, preferred orientation, branching of lamellae and crystal twinning, providing insights about the nucleation mechanism involved in the crystallization of the spherulites. The nucleation starts with a heterogeneous nucleus (pre-existing crystal or bubble) and subsequently it evolves forming “bow tie” morphologies, reaching radially spherulitic shapes in few hours. Since each lamella within spherulite is also twinned, these synthetic spherulites cannot be considered as single nuclei but crystal aggregates originated by heterogeneous nucleation. A twin boundary may have a lower energy than general crystal–crystal boundaries and many of the twinned grains show evidence of strong local bending which, combined with twin plane, creates local sites for heterogeneous nucleation.This study shows that the growth rates of the lamellae (10− 6–10− 7 cm/s) in spherulites are either similar or slightly higher than that for single crystals by up to one order of magnitude. Furthermore, the highest volumetric growth rates (10− 11–10− 12 cm3/s) show that the alkali feldspar within spherulites can grow fast reaching a volumetric size of ~ 10 μm3 in 1 s.
ISSN: 0024-4937

hal-01172356
https://hal.archives-ouvertes.fr/hal-01172356
DOI : 10.1016/j.lithos.2014.12.003

Éditeur(s) : HAL CCSD Mineralogical Society of America
Résumé : International audience
In situ mineralization of CO2 in ultramafic rock-hosted aquifers is one of the promising solutions for decreasing CO2 concentrations in the atmosphere. Naturally altered ultramafic rocks suggest that carbonation processes are controlled by local heterogeneities in the structure of the rock and fluid transport at the water-rock interfaces. We studied the role of rock crystallographic anisotropy relative to the global fluid flow direction on the mineralization of CO2 by means of electron microscope analyses from the macro- to the micrometer scale (EBSD-FIB). The sample used for the measurements was a hot pressed olivine core percolated by water enriched in CO2 (pCO2 = 10 MPa) at 180 °C. During the percolation experiment, olivine was dissolved and two types of carbonates, dolomite, and magnesite, were precipitated on olivine surfaces. The results showed that the dissolution of olivine is controlled by its crystallographic properties as shown by the development of etch-pits only on the (010)ol planes and with elongated shapes parallel to the [010]ol axes. In contrast, the precipitation of carbonates is governed by hydrodynamic properties. Carbonates are heterogeneously distributed in the percolated rock. They are mainly located along the moderate (for dolomite) and the minor (for magnesite) flow paths, both oriented parallel to the principal fluid flow direction, which allow carbonates to be supplied with divalent cations (e.g., Ca2+, Mg2+, and Fe2+). In these flow paths, carbonate growth is systematically oriented normal to the flow that facilitates the development of chemical gradients with cationic supersaturation conditions for carbonate precipitation near the walls.In natural systems, the (010)ol planes are parallel to the Moho and the (100)ol planes are vertical; our study suggests that flow of CO2-rich fluids will induce precipitation of carbonates localized along, and preferentially clogging, vertical flow paths while favoring olivine dissolution along horizontal fluid pathways. This dual control of structure and fluid flow on carbonation mechanisms could be an important parameter allowing sustainable CO2 storage in peridotites, while limiting the risks of leakage toward the surface.
ISSN: 0003-004X

hal-01143393
https://hal.archives-ouvertes.fr/hal-01143393
DOI : 10.2138/am-2015-4913

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
We have inferred the deformation mechanisms of antigorite by high-resolution EBSD mapping of samples from Cerro del Almirez ultramafic massif (Betic Cordillera, SE Spain). Textural relations and phase diagram calculations constrain the foliation development conditions to the subduction prograde path at up to 600-630 °C and 1.6-1.9 GPa. Deformation was followed by static annealing of antigorite at ca. 680 °C. The Crystal Preferred Orientation (CPO) of antigorite is characterised by a strong alignment of (001) poles normal to the foliation plane and a weaker, but clear, parallelism between [100] axes and the macroscopic lineation defined by the elongation of magnetite aggregates. Analysis of misorientations across subgrains shows predominance of [010] rotation axis, consistent with activation of the [100](001) slip system. However, tilt subgrain boundaries subparallel to (100), probably formed by edge dislocations of this system, are subsidiary. Most subgrain boundaries are subparallel to (001) planes. They are interpreted as (001) twins wherein continuing viscoplastic deformation resulted in a slight increase of the misorientation between the twins. Modelling of the evolution of the antigorite CPO using a lower bound approach and considering different deformation regimes and sets of basal and non-basal slip systems has shown that intensities of [100] and [010] maxima reflect the relative strength of the antigorite [100](001) and [010](001) systems. Activation of other basal or non-basal slip systems does not change significantly the CPO patterns, but results in less concentrated CPO. 3D transpression models better reproduce the CPO of natural antigorite serpentinites. We propose that the widespread occurrence of strong CPO in high-pressure antigorite serpentinite is consistent with deformation by dislocation creep with dominant glide on [hk0](001), together with the activation of twinning, implying that a power law rheology would better account for the mechanical behaviour of antigorite serpentinite deep in the subduction channel and mantle wedge.
ISSN: 0012-821X

hal-00795511
https://hal.archives-ouvertes.fr/hal-00795511
DOI : 10.1016/j.epsl.2012.06.049

Éditeur(s) : HAL CCSD Frontiers Media
Résumé : International audience
We present high resolution observations of microstructure and texture evolution during dynamic recrystallization (DRX) of ice polycrystals deformed in the laboratory at high temperature (≈0.98Tm). Ice possesses a significant viscoplastic anisotropy that induces strong strain heterogeneities, which result in an early occurrence of DRX mechanisms. It is therefore a model material to explore these mechanisms. High resolution c-axis measurements at sample scale by optical techniques and full crystallographic orientation measurements by cryo-Electron Back Scattering Diffraction (EBSD) provide a solid database for analyzing the relative impact of the macroscopic imposed stress vs. the local and internal stress fields on DRX mechanisms. Analysis of misorientation gradients in the EBSD data highlights a heterogeneous dislocation distribution, which is quantified by the Nye tensor estimation. Joint analyses of the dislocation density maps and microstructural observations highlight spatial correlation between high dislocation density sites and the onset of nucleation taking place by grain-boundary bulging, subgrain rotation or by the formation of kink-bands.
ISSN: 2296-6463

hal-01515284
https://hal.univ-lorraine.fr/hal-01515284
DOI : 10.3389/feart.2015.00081

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
This paper presents Digital Image Correlation (DIC) and Infrared Thermography (IRT) methods to investigate the thermomechanical behavior of an aluminum at the microstructural scale. Electron BackScattered Diffraction (EBSD) is used to characterize the microstructure of a 3 mm thick specimen with centimetric grain size. This study combines the following imaging techniques: DIC to obtain displacement and strain fields during the test, and IRT to estimate temperature and heat source fields induced by the mechanical loading. Ultimately, the aim of this methodology is to provide energy balance during mechanical test at the scale of the microstructure, in order to propose thermomechanical con-stitutive modelling of crystalline plasticity.
ISSN: 0143-8166

hal-01287711
https://hal.archives-ouvertes.fr/hal-01287711
https://hal.archives-ouvertes.fr/hal-01287711/document
https://hal.archives-ouvertes.fr/hal-01287711/file/Local_experimental_investigations_Li_al_2016.pdf
DOI : 10.1016/j.optlaseng.2016.01.001

Éditeur(s) : HAL CCSD
Résumé : National audience
Les semelles métamorphiques sont situées à la base desgrandes ophiolites obductées. Elles sont principalement composéesd’amphibolites (métabasaltes à amphiboles ± grenat,clinopyroxène, plagioclase) fortement cisaillées et dont les conditionsmaximum de métamorphisme sont estimées à 800±100Cet 1.0±0.2 GPa. Leur formation a lieu au cours des 2 Ma suivantl’initiation des zones de subduction. Ces amphibolites sont interprétéescomme des portions de lithosphère océanique subduite,portions qui sont métamorphisées, dis-je, à haute températurepar transfert de chaleur depuis le coin de manteau sus-jacent quiformera la base de l’ophiolite obductée. Leur importante déformationau pic de métamorphisme est interprétée comme synchroneà leur accrétion au manteau de la plaque supérieure. Les semellesmétamorphiques sont donc des témoins directs de la dynamiqueprécoce des zones de subduction océanique. Leur pétrologie etleur déformation fournissent des contraintes majeures, et rares,sur l’évolution de la structure thermique et sur le comportementmécanique de l‘interface de subduction naissante. Cette étudeprésente des données structurales à plusieurs échelles, couplant desanalyses de terrain aux analyses EBSD sur des échantillons à amphibole± plagioclase ± clinopyroxene ± grenat de la semelle métamorphique.Les grains d’amphibole et de plagioclase sont caractériséspar une forte orientation préférentielle parallèle à la foliationet à la linéation. Cette fabrique est accompagnée par une forteorientation cristallographique préférentielle des amphiboles marquéepar un axe [001] marquant la linéation et la normale au plan(001) perpendiculaire à la foliation. Les plagioclases montrentune orientation cristallographique préférentielle faible voire nulle.Cette fabrique est similaire à celle observée dans les amphibolitescisaillées de base de croûte continentale. Les clinopyroxèneset les grenats présentent des degrés d’orientation intermédiaires.Ces deux phases forment des boudins dont l’axe long est orientéparallèlement à la foliation. Les porphyroclastes de clinopyroxèneprésentent une extinction ondulante et le développement de sousgrainsà leur périphérie. Les clinopyroxènes et les grenats agissentdonc comme phases ” dures ”, augmentant la résistance de laroche à la déformation. À l’initiation de la subduction, la partiesupérieure de la plaque plongeante est affectée par l’augmentationprogressive du degré de métamorphisme. Ceci entraîne une fortedéshydratation et la cristallisation de phases ” faibles ” (quartz,amphibole, plagioclase) et ” fortes ” (clinopyroxene, grenat). Larhéologie de l’interface de la subduction en est fortement affectée.Les unités de la semelle métamorphique (avec des minéralogies etdes conditions P-T-t différentes) accrétées aux péridotites de laplaque supérieure témoignent de changements rhéologiques majeuresà l’interface de la subduction au cours de l’histoire précocedes zones de subduction.
RST 2016, livre des résumés
Caen, France

insu-01388730
https://hal-insu.archives-ouvertes.fr/insu-01388730

Éditeur(s) : HAL CCSD Geological Society of London
Résumé : This paper presents the background for the calculation of physical properties of an aggregate from constituent crystal properties and the texture of the aggregate in a coherent manner. Emphasis is placed on the important tensor properties of 2nd and 4th rank with applications in rock deformation, structural geology, geodynamics and geophysics. We cover texture information that comes from pole figure diffraction and single orientation measurements (electron backscattered diffraction or EBSD, electron channelling pattern, Laue pattern, optical microscope universal-stage). In particular, we provide explicit formulae for the calculation of the averaged tensor from individual orientations or from an orientation distribution function (ODF). For the latter we consider numerical integration and an approach based on the expansion into spherical harmonics. This paper also serves as a reference paper for the mathematical tensor capabilities of the texture analysis software MTEX, which is a comprehensive, freely available MatLab toolbox that covers a wide range of problems in quantitative texture analysis, for example, ODF modelling, pole figure to ODF inversion, EBSD data analysis and grain detection. MTEX offers a programming interface which allows the processing of involved research problems as well as highly customizable visualization capabilities; MTEX is therefore ideal for presentations, publications and teaching demonstrations.
Deformation Mechanisms, Rheology and Tectonics: Microstructures, Mechanics and Anisotropy

hal-00688833
https://hal.archives-ouvertes.fr/hal-00688833

Éditeur(s) : HAL CCSD Springer
Résumé : International audience
Thermoelastic behavior of different marble types was analyzed using computational modeling and experimental measurements. Eight marble samples with different composition, grain size, grain boundary geometry, and texture were investigated. Calcitic and dolomitic marbles were considered. The average grain size varies from 75 μm to 1.75 mm; grain boundary geometry differs from nearly equigranular straight grain boundaries to inequigranular-interlobate grain boundaries. Four typical marble texture types were observed by EBSD measurements: weak texture; strong texture; girdle texture and high-temperature texture. These crystallographic orientations were used in conjunction with microstructure-based finite element analysis to compute the thermoelastic responses of marble upon heating. Microstructural response maps highlight regions and conditions in the marble fabric that are susceptible to degradation phenomena. This behavior was compared to the measured thermal expansion behavior, which shows increasing residual strains upon repetitive heating-cooling cycles. The thermal expansion behavior as a function of temperature changes can be classified into four categories: (a) isotropic thermal expansion with small or no residual strain; (b) anisotropic thermal expansion with small or no residual strain; (c) isotropic thermal expansion with a residual strain; and (d) anisotropic thermal expansion with residual strain. Thermal expansion coefficients were calculated for both simulated and experimental data and also modeled from the texture using the MTEX software. Fabric parameters control the amount and directional dependence of the thermal expansion. Marbles with strong texture show higher directional dependence of the thermal expansion coefficients and have smaller microstructural values of the maximum principal stress and strain energy density, the main precursors of microcracking throughout the marble fabric. In contrast, marbles with weak texture show isotropic thermal expansion behavior, have a higher propensity to microcracking, and exhibit higher values of maximum principal stress and strain energy density. Good agreement between the experimental and computational results is observed, demonstrating that microstructure-based finite-element simulations are an excellent tool for elucidating influences of rock fabric on thermoelastic behavior.
ISSN: 1866-6280

hal-00858095
https://hal.archives-ouvertes.fr/hal-00858095
DOI : 10.1007/s12665-013-2406-z

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
Prediction of ice mass flow and associated dynamics is pivotal at a time of climate change. Ice flow is dominantly accommodated by the motion of crystal defects – the dislocations. In the specific case of ice, their observation is not always accessible by means of the classical tools such as X-ray diffraction or transmission electron microscopy (TEM). Part of the dislocation population, the geometrically necessary dislocations (GNDs) can nevertheless be constrained using crystal orientation measurements via electron backscattering diffraction (EBSD) associated with appropriate analyses based on the Nye (1950) approach. The present study uses the Weighted Burgers Vectors, a reduced formulation of the Nye theory that enables the characterization of GNDs. Applied to ice, this method documents, for the first time, the presence of dislocations with non-basal or Burgers vectors. These or dislocations represent up to of the GNDs observed in laboratory-deformed ice samples. Our findings offer a more complex and comprehensive picture of the key plasticity processes responsible for polycrystalline ice creep and provide better constraints on the constitutive mechanical laws implemented in ice sheet flow models used to predict the response of Earth ice masses to climate change.
ISSN: 0012-821X

hal-01685565
https://hal.archives-ouvertes.fr/hal-01685565
DOI : 10.1016/j.epsl.2017.06.020

Éditeur(s) : HAL CCSD Geological Society of London
Résumé : International audience
The mylonitic Cambrian quartzites, Moine Thrust Zone, NW Scotland, have long been used to study microstructural and petrofabric evolution and to develop understanding of grain-scale processes accommodating large-scale displacements. Today, structural geology is entering a new age of understanding of the basic processes involved in microstructural evolution due to the emergence of novel instrumental techniques and theoretical models. It seems apposite therefore to re-evaluate the microstructure of one example of this classic quartz mylonite from the Stack of Glencoul, Assynt, using arguably the most important of these new techniques, electron backscattered diffraction (EBSD). The three-dimensional (3D) microstructure and petrofabric of this rock was analysed using EBSD, to: 1) corroborate previous optical and X-ray texture goniometry measurements; 2) investigate the potential for sampling and/or tectonic sectioning bias that may be introduced inadvertently into any petrofabric analysis; and 3) predict its seismic properties. It is found that microstructures do differ between orthogonal structural sections, leading to variations in strengths of different components in the overall petrofabric that might impact on seismic properties. The results emphasize the true 3D nature of microstructures and petrofabrics, which can be recognized and accommodated more readily by this new generation of analytical techniques.
Continental Tectonics and Mountain Building: The Legacy of Peach and Horne

hal-00565749
https://hal.archives-ouvertes.fr/hal-00565749

Éditeur(s) : HAL CCSD Trans Tech Publications Inc.
Résumé : Two, high purity, Al-0.1 and 0.3wt%Mn alloys have been cold deformed in plane strain compression to strains of order 1.8 and the kinetics of subsequent recovery by sub-grain coarsening during annealing at 150-300°C measured by high resolution FEG-SEM EBSD. Accurate sub-grain size and misorientation distributions and their evolution with time and temperature have been determined. The average growth rates are then used to estimate the sub-grain boundary mobilities. Growth is analyzed by two well-known growth laws for the average sub-grain size δ (t): i) the standard relation for grain growth: where the exponent n takes values of 2-8 and ii) the relation proposed by Nes for dislocation climb in sub-grain walls: It is shown that the latter relation gives a better fit with the data in terms of the time and temperature dependence of the sub-grain sizes. In particular the activation energies for the logarithmic law are much closer to the values expected for solute-controlled movement of sub-boundaries.
Materials Science Forum

hal-00795441
https://hal.archives-ouvertes.fr/hal-00795441
DOI : 10.4028/www.scientific.net/MSF.715-716.725

Éditeur(s) : HAL CCSD
Résumé : National audience
Un ensemble de données sur l’environnement géologique despéridotites de la Zone Nord-Pyrénéenne a été obtenu dans lecadre des programmes ANR Pyramid et RGF-BRGM consacrésà l’évolution géodynamique des Pyrénées. Ces données représententdes contraintes indispensables pour l’étude des processus del’exhumation du manteau, de l’amincissement de la croûte continentaleet de sa disparition complète lors de l’ouverture desbassins transtensifs albo-cénomaniens. On y trouve : (1) de nouveauxlevés géologiques de détail autour des lherzolites de Lherz-Freychinède-Vicdessos-Bestiac-Prades et d’Urdach-Les Pernes et(2) des analyses multi-méthodes des métasédiments de la couvertureprérift et du socle paléozoïque adhérent au manteau :composition des assemblages du métamorphisme HT, températuresmaximales par spectrométrie RAMAN sur la m.o., fabriquede la calcite par EBSD, inclusions fluides et isotopes stables dansles marbres et veines associées, datations U-Th-Pb in situ. Cesdonnées permettent d’estimer les conditions thermiques lors de laremontée du manteau et de sa mise à l’affleurement. Nous montronsune variabilité remarquable de l’Ouest vers l’Est.A l’Ouest, le manteau est exhumé à l’Albien sup. - Cénomanieninf. en perçant une couverture mésozoïque prérift qui n’a pas étéchauffée à plus de 250C. La croûte continentale supérieure y estréduite en lames ductiles extrêmement amincies puis cataclaséeset remaniées sur le fond ultrabasique avec des fragments de manteauet de la couverture prérift, durant le dépôt du flysch noir. Latempérature augmente au cours du Cénomanien (480C) dans leszones où le manteau n’a pas été mis à l’affleurement. Le Triassupérieur se transforme profondément (talc-chlorites) et perd sacomposante évaporitique. La couverture prérift décollée joue unrôle majeur comme couvercle isotherme, suivi en cela par les flyschsalbiens puis cénomaniens.A l’Est, le manteau perce à travers une couverture chauffée localementà plus de 600C. Le Keuper y est réduit à quelquesdécimètres de grès et brèches riches en saphirine. La croûtesupérieure a été presque totalement éliminée tectoniquement, maisdes granulites sont remaniées à côté des péridotites et des marbresdans les brèches recouvrant le manteau exhumé.Ces données de terrain représentent les contraintes de base pourconstruire les modèles d’amincissement crustal. La variabilitémise en évidence (gradient thermique et présence ou absence decroûte profonde remaniée) ne permet pas de proposer un modèled’amincissement simple et unique. Cependant, toutes ces donnéesindiquent que la croûte moyenne à supérieure se comporteductilement sous les écrans thermiques de la couverture prériftet synrift, mobiles sur le Keuper. Un modèle de marge passivedistale faisant appel à des blocs continentaux rigides de type ”extensional allochthons ” ne peut s’appliquer ici. Sur la base deces données géologiques, nous mettons donc en avant un nouveaumodèle de type marge distale chaude plus ou moins transtensive.
RST 2016, livre des résumés
Caen, France

insu-01388463
https://hal-insu.archives-ouvertes.fr/insu-01388463

Éditeur(s) : HAL CCSD Elsevier
Résumé : We have studied the phase transformation of forsterite to wadsleyite under shear stress at the Earth's transition zone pressure and temperature conditions. Two-step experiments were performed using a multi-anvil press. First, we hot pressed iron-free forsterite at 6 or 11 GPa and 1100 degrees C. Then we deformed a slab of this starting material using a direct simple shear assembly at 16 GPa and 1400 degrees C for 1, 15, 35, 40, or 60 min. Both the starting material and the deformed samples were characterized using optical and scanning electron microscopy including measurements of crystal preferred orientations (CPO) by electron back scattered diffraction (EBSD), transmission electron microscopy (TEM), and Fourier transform infrared spectroscopy (FTIR). The phase transformation occurs very rapidly, in less than 1 min, and metastable forsterite relics are not observed after deformation. The grain size of wadsleyite is slightly smaller than the forsterite starting material. The water contents obtained from FTIR analyses in forsterite and wadsleyite are 65-124 wt ppm H2O and 114-736 wt ppm H2O, respectively, which are well below water solubility at similar conditions in the presence of free water. Wadsleyite aggregates display weak CPO patterns with [1 0 0] axes concentrated at low angle to the shear direction, [0 1 0] axes perpendicular to the shear plane and nearly random [0 0 1] axes. Only a few dislocations were observed in wadsleyite with TEM. This observation is consistent with the assumption that most dislocations formed during the initial high-stress stages of these stress-relaxation experiments, were consumed in the phase transformation, probably enhancing the transformation rate. CPO patterns vary as a function of the water content: with increasing water content the density of [1 0 0] axes parallel to the shear direction decreases, and the density of [0 0 1] axes increases. Viscoplastic self-consistent modeling of CPO evolution using previously reported glide systems for wadsleyite, i.e., [1 0 0]{0 k 1} and 1/2 (1 1 1){1 0 1}, cannot reproduce the measured CPO, unless the [0 0 1](0 1 0) system, for which dislocations have not been observed by TEM, is also activated. In addition, wadsleyite grain growth suggests the participation of diffusion-assisted processes in deformation. Calculated anisotropies for P and S-waves using measured CPO are always below 1%. This very low anisotropy is due to both the low finite strain achieved in the experiments, which leads to weak wadsleyite CPO, and to the diluting effect of added majorite. The present experiments emphasize the importance of stress, grain size evolution and water content in the forsterite to wadsleyite phase transformation and subsequent deformation in the transition zone.
ISSN: 0031-9201

hal-00617430
https://hal.archives-ouvertes.fr/hal-00617430
DOI : 10.1016/j.pepi.2010.11.001

Éditeur(s) : HAL CCSD
Résumé : International audience
The influence of Mn solute atoms on sub-grain boundary mobilities in Al has been determined by accurate electron backscatter diffraction analysis of the sub-grain sizes and misorientations during recovery annealing. High purity Al-0.1 and 0.3 wt.% Mn alloys were deformed by plane strain compression at room temperature to equivalent strains of 1.8 and annealed in the temperature range 150-300 °C. An original method of image analysis on sub-boundaries from electron backscatter diffraction maps was applied to quantify the sub-grain size distributions. The change in average sub-grain size with time at several temperatures was then used to estimate sub-grain boundary mobilities in both Al-Mn alloys. The activation energies for sub-grain mobility were found to be 48 and 52 and kJ.mol^-1 for the 0.1 and 0.3 % Mn alloys respectively, with the higher Mn alloy exhibiting lower rates. The sub-boundary mobilities are higher than expected from previous similar work on deformed Al-Si crystals. The orientation dependence of sub-grain growth is also examined.
International Journal of Materials Research

emse-00463551
https://hal-emse.ccsd.cnrs.fr/emse-00463551
DOI : 10.3139/146.110057

Éditeur(s) : HAL CCSD
Résumé : International audience
Metamorphic soles correspond to m to 500 m thick highly strained metamorphic rock units found beneath myloniticbanded peridotites at the base of large-scale ophiolites, as exemplified in Oman. Metamorphic soles aremainly composed of metabasalts deriving from the downgoing oceanic lithosphere and metamorphosed up togranulite-facies conditions by heat transfer from the mantle wedge. Pressure–temperature peak conditions areusually estimated at 1.00.2 GPa and 800100ºC. The absence of HP–LT metamorphism overprint implies thatmetamorphic soles have been formed and exhumed during subduction infancy. In this view, metamorphic soleswere strongly deformed during their accretion to the mantle wedge (corresponding, now, to the base of the ophiolite).Therefore, metamorphic soles and banded peridotites are direct witnesses of the dynamics of early subductionzones, in terms of thermal structure, fluid migration and rheology evolution across the nascent slab interface.Based on fieldwork and EBSD analyses, we present a detailed (micro–) structural study performed on samplescoming from the Sumeini window, the better-preserved cross-section of the metamorphic sole of Oman. Largedifferences are found in the deformation (CPO, grain size, aspect ratio) of clinopyroxene, amphibole and plagioclase,related to mineralogical changes linked with the distance to the peridotite contact (e.g., hardening due to theappearance of garnet and clinopyroxene).To model the incipient slab interface in laboratory, we carried out 5 hydrostatic annealing and simple-shear experimentson Griggs solid-medium apparatus. Deformation experiments were conducted at axial strain rates of 10-6s-1. Fine-grained amphibolite was synthetized by adding 1 wt.% water to a (Mid-Ocean Ridge) basalt powder asa proxy for the metamorphic sole (amphibole + plagioclase + clinopyroxene garnet assemblage). To synthetizegarnet, 2 experiments were carried out in hydrostatic conditions and with deformation at 800C with confiningpressure of 2 GPa. Another simple-shear experiment has been carried out at 800C and 1 GPa with fined-grainednatural garnet. With the aim of mimicking the early slab interface (between the metamorphic sole and bandedperidotites at the base of the ophiolite), 2 simple-shear deformation experiments with 2 layers have been carriedout at 800C and confining pressure of 1 GPa. The bottom layer was made of hydrated basalt powder and the toplayer was made of olivine.Fined-grained garnet-free amphibolite is significantly weaker than dunite but the appearance of harder mineralsin the amphibolite (garnet and clinopyroxene) has major implications on its rheological evolution. These resultsallow liking field observations of strain localization at the interface to the metamorphic sole formation
European Geosciences Union General Assembly 2016
Vienne, Austria

insu-01309394
https://hal-insu.archives-ouvertes.fr/insu-01309394

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
Microstructures, U-Pb SHRIMP zircon ages and temperature estimates were used to constrain the fabric evolution and timing of mylonitisation in the Patos shear zone (NE Brazil). Melt-bearing HT-mylonitic orthogneiss displays solid-state fabrics with coarse quartz ribbons and sutured grain boundaries. K-feldspar is often fractured and shows peripheral myrmekite. The textures typically become magmatic at the contacts with the Espinho Branco anatexite. Zircon crystals from two samples of the leucosome show Paleoproterozoic (ca. 2.2 Ga) inherited cores that are enveloped by recrystallised Neoproterozoic rims. These zircon grains define a discordia with lower intercept ages of 558 and 562 Ma but with large analytical errors. A leucogranite with transitional contacts with host diatexites provides a well-constrained zircon mean age of 566 ± 6 Ma (n = 15, 95% conf.), which is considered the best estimate for the peak metamorphic conditions. The transition from HT-mylonites to fine-grained mylonites and ultramylonites is marked by a progressive grain size reduction assisted by recrystallisation. Quartz crystallographic fabrics display [0 0 0 1] concentrations between Z and Y. K-feldspar and plagioclase fabrics record the activity of the (0 1 0)[0 0 1] and (0 1 0)[1 0 0] slip systems and, in the lower-temperature tectonites, the (1 0 0)[0 1 0] slip system. These results suggest a diachronic evolution in which an initial HT northern domain was deformed by intracrystalline slip and melt-assisted granular flow, followed by medium- to low-temperature solid-state creep in the southern shear zone domain. The mylonites therefore record the rheological heterogeneities responsible for the formation of a late continental shear zone that nucleated under partially molten conditions and was later reactivated through melt-absent strain localization following exhumation.
ISSN: 0301-9268

hal-01053497
https://hal.archives-ouvertes.fr/hal-01053497
DOI : 10.1016/j.precamres.2013.12.020