Éditeur(s) : HAL CCSD Springer/Terra Scientific Publishing Company
Résumé : International audience
We report oil the discovery of magnetite nanoparticles ranging in size from 2 to 14 full in the mineralized zones of the Pena Colorada iron-ore deposit, southern Mexico. Micrometric scale magnetite was magnetically reduced and divided into distinct size ranges: 85-56 mu m, 56-30 mu m, 30-22 mu m, 22-15 mu m, 15-10 mu m, 10-7 mu m and 7-2 mu m. Nanometric-scale magnetite in the size range 2-14 nm was identified. The magnetite was characterized by X-ray diffraction, transmitted and reflected light microscope, high-resolution transmission electron microscopy (TEM), high angle annular dark field, Mossbauer spectroscopy and its magnetic properties. Crystallographic identification of nanostructures Was performed using high-resolution TEM. Characteristic changes were observed when the particles make the size transition from micro- to nanometric sizes, as follows: (1) frequency-dependent magnetic Susceptibility percentage (chi FD%) measurements Show high Values (13%) for the 2-14 nm fractions attributed to dominant fractions of superparamagnetic particles; (2) variations of chi FD% < 4.5% in fractions of 56-0.2 mu m occur in association with the presence of microparticles formed by magnetite aggregates of nanoparticles (< 15 nm) embedded in berthierine; (3) Mossbauer spectroscopy results identified a superparamagnetic fraction; (4) nanometric and 0.2-3 mu m grain size magnetite particles require a magnetic field up to 152 mT to reach saturation during the isothermal remanent magnetization experiment; (5) coercivity and remanent magnetization of the magnetite increase when the particle size decreases, probably due to parallel Coupling effects; (6) two-magnetic Susceptibility versus temperature experiments of the same 2-14 nm sample show that the reversibility during the second heating is due to the formation of new magnetite nanoparticles and growth of those already present. during the first heating process.
ISSN: 1343-8832

hal-00413053
https://hal.archives-ouvertes.fr/hal-00413053

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
A detailed rock-magnetic and archeointensity study was carried out on materials baked by a western Mexican artisan following traditional techniques to produce faithful reproductions of archeological pieces of the Michoacan region (Western Mesoamerica). The field strength at the site (41.0 +/- 0.51 mu T) was measured with a fluxgate magnetometer and the temperature of the furnace during the baking process was monitored continually by means of a thermocouple placed in the middle of the baking cavity.;Rock-magnetic experiments performed on the raw material (clay and paste) and on in situ prepared baked ceramics and bricks included measurement of thermomagnetic curves (susceptibility and strong-field magnetization versus temperature), first-order reversal curves (FORC), anisotropy of magnetic susceptibility (AMS) and anisotropy of thermoremanent magnetization (A-TRM). Magnetite and probably hematite are present in the samples as carriers of the remanence. Hysteresis ratios suggest that the samples fall in the pseudo-single-domain grain size region, which may indicate a mixture of multidomain and a significant amount of single-domain grains.;Ceramic pieces and brick fragments were subjected to the Thellier-Coe archeointensity method and to an alternative paleointensity experiment, with a TRIAXE magnetometer, in order to check whether they are faithful recorders of the local geomagnetic field strength.;Mean raw-intensity of sample M1 (pottery) overestimates a 7% the expected site intensity, while those corresponding to the brick samples (LQ1 and LQ2) underestimate it 15%. Brick sample LNQ shows a slightly lower intensity (7%), but agrees with the expected site intensity within the experimental uncertainty. The intensity retrieved from the volcanic fragment also included closely reproduces the expected intensity. After A-TRM and cooling-rate corrections, all mean raw values move closer to the expected intensity.;Measurement of temperatures at different parts inside the kiln (bottom and upper parts of both central and peripheral parts) revealed the existence of significant thermal gradients, similar to those observed in ovens from other localities. Different cooling rates are then expected in a single oven.;The scatter in the intensity determinations observed in this study, retrieved from pieces elaborated together in the same oven, could arise from this differentiated cooling rate within the oven and thus, to an inappropriate cooling rate correction in the archeointensity protocol. As this situation was probably reproduced in the baking of ancient ceramic artifacts, a better knowledge of the temperature distribution inside these types of kiln would be desirable in order to choose the appropriate cooling rate correction.
ISSN: 0031-9201

hal-00644559
https://hal.archives-ouvertes.fr/hal-00644559
DOI : 10.1016/j.pepi.2011.06.007

Éditeur(s) : HAL CCSD Springer Verlag (Germany)
Résumé : International audience
The influence of magnetic interactions on the anisotropy of magnetic susceptibility (AMS) have been largely studied by several theoretical models or experiments. Numerical models have shown that when magnetostatic interactions occur, the distributions of particles over the volume rather than their individual orientations control the AMS. We have shown recently from a comprehensive rock magnetic study and from a theoretical 2-dimensional (2-D) model that single domain particles closely packed in globule aggregates could produce strong local random interaction magnetic fields which could influence the magnetic susceptibility and decrease the degree of anisotropy. In this paper, we first present in detail this 2-D theoretical model and then we extend it to the 3-D case. The possible distribution function of the magnetostatic interaction fields comprises two extreme states: it is either isotropic or ordered. The former case corresponds to the thermal-demagnetized state while the second case corresponds to the alternating field (AF) demagnetized state. We show that when easy axes of magnetization are not uniformly distributed, the degree of anisotropy decreases as the interaction field increases in both AF- and thermal-demagnetized states in 2-D and 3-D geometry. Thus we conclude that random magnetic fields generated by a random arrangement of magnetic particles over the sample volume decrease the degree of anisotropy of AMS and may alter the magnetic fabric.
ISSN: 0039-3169

hal-00758113
https://hal.archives-ouvertes.fr/hal-00758113
https://hal.archives-ouvertes.fr/hal-00758113/document
https://hal.archives-ouvertes.fr/hal-00758113/file/SGEG-2012-HAL.pdf
DOI : 10.1007/s11200-010-9097-7

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
This work combines structural and geochronological data to improve our understanding of the mechanical behaviour of continental crust involving large amount of magma or partially melted material in an abnormally hot collisional belt. We performed a magnetic and geochronological (U/Pb) study on a huge tonalitic batholith from the Neoproterozoic Araçuaí belt of East Brazil to determine the strain distribution through space and time. Anisotropy of magnetic susceptibility, combined with rock magnetism investigations, supports that the magnetic fabric is a good proxy of the structural fabric. Field measurements together with the magnetic fabrics highlight the presence in the batholith of four domains characterized by contrasted magmatic flow patterns. The western part is characterized by a gently dipping, orogen-parallel (∼NS) magmatic foliation that bears down-dip lineations, in agreement with westward thrusting onto the São Francisco craton. Eastward, the magmatic foliation progressively turns sub-vertical with a lineation that flips from sub-horizontal to sub-vertical over short distances. This latter domain involves an elongated corridor in which the magmatic foliation is sub-horizontal and bears an orogen-parallel lineation. Finally the fourth, narrow domain displays sub-horizontal lineations on a sub-vertical magmatic foliation oblique (∼N150°E) to the trend of the belt. U/Pb dating of zircons from the various domains revealed homogeneity in age for all samples. This, together with the lack of solid-state deformation suggests that: 1) the whole batholith emplaced during a magmatic event at ∼580 Ma, 2) the deformation occurred before complete solidification, and 3) the various fabrics are roughly contemporaneous. The complex structural pattern mapped in the studied tonalitic batholith suggests a 3D deformation of a slowly cooling, large magmatic body and its country rock. We suggest that the development of the observed 3D flow field was promoted by the low viscosity of the middle crust that turned gravitational force as an active tectonic force combining with the East-West convergence between the São Francisco and Congo cratons.
ISSN: 0191-8141

hal-00745696
https://hal.archives-ouvertes.fr/hal-00745696
DOI : 10.1016/j.jsg.2012.02.015

Éditeur(s) : HAL CCSD
Résumé : The Earth's magnetic field shows a large range of temporal variations from the year to several million years. I studied during my PhD thesis several aspects of these fluctuations, from recent secular variations to reversals. The first part of my manuscript deals with archeomagnetism, a discipline that allows to track the temporal variations of the Earth's magnetic field through millennia, mainly from archeological materials. I studied two sets of samples , one from Greece (Neolithic period 6800-3200 B.C.) and the other from Mexico (Palenque, Maya Classic period 320-840 A.D.), to acquire new archeointensity data in order to better constrain the secular variation of the geomagnetic field. By comparing my data with those available in the literature and with the various global and regional models, I showed that the secular variations during the Neolithic in Greece and during the first millennium in Central America are poorly defined. My data suggest that local components, not described by global models, may exist in these regions. They reinforce the importance of developing specific regional models. As a consequence, the acquisition of new high quality data is of main importance. The second part presents the description of a geomagnetic field reversal. This work was based on two points : first by studying transitional directions to provide new constraints on the possible preferred longitudinal paths of virtual geomagnetic poles (VGPs) and second by checking transitional paleointensities obtained on a volcanic sequence in Akaroa volcano (New Zealand). Indeed the transitional field intensity is significantly higher than the field intensity before and after the reversal. We re-sampled this sequence, and the directional results show a complex sequence of N-T-R-T-N-T-R polarity. The transitional VGPs obtained are clustered in two longitudinal bands through Australia and America. This observation seems to reinforce the assumption of a core-mantle interaction over several million years. Following a rock magnetic study, I selected samples that could provide a value for the Thellier and multispecimen paleointensity methods. The obtained paleointensity are relatively low (about 20 μT) during the polarity change and strong at the end of the sequence. Based both on the field strength values and on the radiochronological ages, showing that the sequence was erupted in a very short time, I suggest that only the C4AR.1n-C4Ar.1r reversal was recorded in this sequence. In this assumption, the reversal shows a complex path comparable to other reversals recorded in the northern hemisphere (for example the Steens Mountain ), including a rebound before stabilizing. Finally the last part is devoted to the development of a new methodology and a new apparatus to determine absolute paleointensity. Following the low success rate of paleointensity experiments from the previous study, I decided to test the multispecimen protocol, which can be applied to samples yielding a predominant multidomaine behavior. The main technical drawback of this method lies in the application of the laboratory field along the natural remanent magnetization, a difficult task to perform accurately in standard paleointensity ovens. Thus, we decided to adapt sample holders from our standard oven in order to allow the sample orientation in space and to develop an ultra-fast heating oven prototype particularly well-suited for this method, allowing to apply the laboratory field in the 3 dimensions. I checked the different multispecimen protocols on historical lavas from Reunion and Etna volcano, yielding very different magnetic mineralogies. For all flows, I obtained paleointensities very close from the expected values, regardless from the magnetic mineralogy, revealing the feasibility of our apparatus and the promising interest of the method. The application of various corrections on the statistical estimation of the intensity value or on the cooling rate had no significant impact on my results.
La première partie de ma thèse porte sur l'archéomagnétisme, discipline qui permet de retracer l'évolution temporelle du champ magnétique terrestre au travers des derniers millénaires, principalement à partir des matériaux archéologiques. J'ai étudié deux jeux d'échantillons provenant pour l'un de la Grèce (période néolithique, 6800-3200 avant J.C.) et pour l'autre du Mexique (Palenque, période Maya Classique 320-840 après J.C.), dans le but d'acquérir de nouvelles données d'archéointensité et de mieux contraindre la variation séculaire du champ magnétique terrestre. La comparaison de mes données avec celles disponibles dans la bibliographie et avec les différents modèles globaux et régionaux a mis en évidence que les variations séculaires au Néolithique en Grèce et au cours du premier millénaire en Amérique Centrale sont très mal définies. Mes données suggèrent que des composantes locales, non prisent en compte dans les modèles globaux peuvent exister au niveau de ces régions. Elles renforcent l'intérêt de développer des modèles régionaux précis. Pour ce faire, l'acquisition de nouvelles données de haute qualitéest un élément majeur. La deuxième partie traite de la description d'un renversement du champ magnétique terrestre. Cette étude a été basée sur deux points précis : étudier les directions transitionnelles afin d'apporter de nouvelles contraintes sur le possible confinement longitudinal des pôles géomagnétiques virtuels (PGV) d'une part, et d'autre part vérifier des paléointensités transitionnelles obtenues sur la séquence volcanique d'Akaroa (Nouvelle Zélande), dont l'intensité est significativement supérieure à celles des intensités avant et après le renversement. Nous avons ré-échantillonné cette séquence, et l'évolution directionnelle obtenue pour ce renversement est une succession complexe de polarités N-T-R-T-N-T-R. Les PGV obtenus semblent se regrouper sous deux bandes longitudinales sous l'Australie et l'Amérique, ce qui renforce l'hypothèse d'une interaction entre le manteau et le noyau sur plusieurs millions d'années. Suite à une étude de minéralogie magnétique, j'ai sélectionné les échantillons susceptibles de fournir une valeur de paléointensité par les méthodes de Thellier et du multispecimen. Les paléointensités obtenues sont relativement faibles (environ 20 μT) au cours du changement de polarité et forte à la fin de la séquence. Mon interprétation, basée à la fois sur les valeurs de l'intensité du champ et sur les données radiochronologiques montrant que la séquence s'est mise en place très rapidement, est de considérer que seul le renversement C4Ar.1n-C4Ar.1r a été enregistré dans cette séquence. Dans cette hypothèse, le renversement montre un cheminement complexe comparable à d'autres renversements enregistrés dans l'hémisphère nord (comme celui de la Steens Mountain par exemple), incluant un phénomène de rebond avant de se stabiliser. La troisième partie de ma thèse est consacrée au développement d'une nouvelle méthodologie et d'un nouvel appareillage pour déterminer des paléointensités. Le faible taux de réussite des expériences de paléointensité de l'étude précédente m'a poussé à m'intéresser au protocole multispecimen, qui peut s'appliquer aux échantillons possédant un comportement polydomaine. L'inconvénient technique majeur de cette méthode réside dans l'application du champ le long de l'aimantation naturelle, difficile à réaliser avec précision dans les fours standards. Pour ce faire, nous avons décidé de développer des porte-échantillons permettant d'orienter les échantillons dans l'espace pour le four standard et un prototype de four à chauffage ultra-rapide particulièrement bien adapté avec la possibilité d'orienter le champ appliqué dans les 3 dimensions. J'ai testé les différents protocoles de la méthode sur des laves historiques de la Réunion et de l'Etna, possédant des minéralogies très différentes. Pour l'ensemble des coulées étudiées, j'ai obtenu des paléointensités très proches des valeurs attendues, et ce indépendamment de la minéralogie, révélant ainsi le faisabilité de notre appareillage et le côté prometteur de la méthode. L'application de diverses corrections sur la statistique d'estimation de la valeur de l'intensité ou sur le taux de refroidissement n'ont eu aucun impact notable sur mes résultats.
https://tel.archives-ouvertes.fr/tel-00719380

tel-00719380
https://tel.archives-ouvertes.fr/tel-00719380
https://tel.archives-ouvertes.fr/tel-00719380/document
https://tel.archives-ouvertes.fr/tel-00719380/file/thesefanjat2012.pdf

Éditeur(s) : HAL CCSD Geological Society of London
Résumé : The Zagros Simply Folded Belt (ZSFB) is an active fold-and-thrust belt resulting from the still continuing continental collision between the Arabian plate and the Iranian plate, which probably started in the Oligocene. The present-day shortening (N25°) is well documented by focal mechanisms of earthquakes and global positioning system (GPS) surveys. We propose in this study a comparison of published palaeostress markers, including magnetic fabric, brittle deformation and calcite twinning data. In addition, we describe the magnetic fabric from Palaeocene carbonates (10 sites) and Mio-Pliocene clastic deposits (15 sites). The magnetic fabrics are intermediate, with magnetic foliation parallel to the bedding, and a magnetic lineation mostly at right angles to the shortening direction. This suggests that the magnetic fabric retains the record of an early layer-parallel shortening (LPS) that occurred prior to folding. The record of LPS allows the identification of originally oblique folds such as the Mand Fold, which have developed in front of the Kazerun Fault. The shape parameter of the magnetic fabric indicates a weak strain compatible with the development of detachment folds in the ZSFB. The palaeostress datasets, covering the Palaeocene to Pleistocene time interval, support several folding episodes accompanied by a counter-clockwise rotation of the stress field direction. The Palaeocene carbonates in the ZSFB record a N47 LPS during early to middle Miocene detachment folding in the High Zagros Belt (HZB). The Mio-Pliocene clastic deposits recorded a N38 LPS prior to and during detachment folding within the ZSFB at the end of the Miocene-Pliocene. Similarly, fault slip and calcite twin data from the ZSFB also support a counter-clockwise rotation from NE to N20 between the pre-folding stage and the late rejuvenation of folds. This counter-clockwise trend of palaeostress data agrees with fault slip data from the HZB. During the late stage of folding in the ZSFB, the Plio-Quaternary palaeostress trends are consistently parallel to the present-day shortening direction.
Tectonic and stratigraphic evolution of Zagros and Makran during the Mesozoic-Cenozoic

hal-00545036
https://hal.archives-ouvertes.fr/hal-00545036
DOI : 10.1144/SP330.6

Éditeur(s) : HAL CCSD Oxford University Press (OUP)
Résumé : International audience
Anisotropy of low-field magnetic susceptibility (AMS) of basaltic lava flows can give some clues about post-emplacement tilting occurring in volcanic sequences. Such a study has been carried out on a sequence of 19 successive lava flows from Kerguelen Archipelago. Surprisingly, two different patterns were observed. The first one - herein called normal fabric - is consistent with the lava-flow direction inferred from geological observations, whereas the second one observed for about 70 per cent of the analysed samples - herein called abnormal fabric - appears to be unrelated to the shear history of the lava flows during their emplacements. These abnormal fabrics are not strictly inverse fabric but seem to have a more complex origin. The unusual nature of these abnormal fabrics has been confirmed by lattice preferred orientation of plagioclases obtained from high-resolution electron backscattered diffraction measurements. The aim of this study is to propose a physical interpretation of these fabrics. A first step in our understanding was to clearly identify the nature and the magnetic properties of the Fe-Ti oxides assemblage. Thus, we present a comprehensive rock magnetic analysis relying on low- and high-temperature thermomagnetic curves (K-T), crossover diagrams, first-order reversal curves, ore-microscopy, Mössbauer measurements and electron backscattered images. We found that in the present case the abnormal fabrics are probably linked to a mixture of prevailing single domain (SD) strongly interacting grains population and a subsidiary multidomain grains population. SD grains are identified as small magnetite crystallized within the interstitial glass in globular aggregates along the silicate framework. Then a question arises: to what extent such SD interacting grains in globular aggregates can affect the magnetic susceptibility and its anisotropy? To answer this question, we developed a physical model in which the total energy density of an SD grain with an uniaxial anisotropy is minimized. In this model, the distribution function of the direction of the magnetic interaction field is comprised between two boundary states. It is either isotropic, which formally corresponds to the thermal demagnetized state, or it is ordered, which formally corresponds to the Alternative Field demagnetized state. We show that in both cases the degree of anisotropy decreases as the interaction field increases. Thus, we conclude that the abnormal fabric encountered in this study can be simply explained by strong magnetostatic interactions that would explain the large scattering of AMS often observed in basaltic lava flows.
ISSN: 0956-540X

hal-00716449
https://hal.archives-ouvertes.fr/hal-00716449
https://hal.archives-ouvertes.fr/hal-00716449/document
https://hal.archives-ouvertes.fr/hal-00716449/file/gji-S-12-HAL.pdf
DOI : 10.1111/J.1365-246X.2012.05421.X

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
Mechanism and kinematics of the Late Mesozoic continental extension event of eastern Asia are still debated. In order to better constrain its evolution, two granodioritic plutons of the Jiaodong Peninsula have been chosen as targets for a time-constrained palaeomagnetic study. Indeed, plutons are devoid of visible deformation, did not experience rotation along horizontal axis and are precisely dated by U/Pb and 40Ar/39Ar methods. Multidomain (MD) magnetite has been identified as the principal magnetic remanent carrier. The interpolation of existing and new U/Pb and 40Ar/39Ar ages revealed that characteristic remanent magnetisation was acquired in a narrow range of 116 ± 2 Ma. Twenty out of 27 sites present stable magnetic directions calculated from high-temperature or high-coercive components. The observations of the solo normal magnetic polarity for this palaeomagnetic collection and of the magnetic remanent age consistent with the Cretaceous Normal Superchron (CNS) argue that the characteristic magnetic remanence may be considered as primary. Detailed field observations of the intrusive relationship between the plutons and country rocks and Anisotropy of Magnetic Susceptibility (AMS) study reveal the absence of the subsequent deformation of plutons, or rigid rotation of plutons along a horizontal axis. Two palaeomagnetic poles have been therefore calculated from these plutons. Among 12 out 15 Cretaceous palaeomagnetic poles, including the two new poles provided by this study, from the Jiaodong Peninsula and on both sides of Tan-Lu and Muping-Jimo faults are statistically consistent. As a result, the Jiaodong Peninsula behaved as a rigid block as internal deformation appears negligible. The remaining three derived poles are probably due to the secular variation or/and the vicinity of fault zones near of the palaeomagnetic sampling site. Thus, they can not be applied to the peninsula-scaled tectonics. Comparison of these time52 constrained Cretaceous palaeomagnetic results of the Jiaodong Peninsula with those of North China Block (NCB) indicate that the Jiaodong Peninsula was rigidly attached to NCB since, 3 at least, the Cretaceous as residual difference is clearly insignificant with respect to the error brackets. These new palaeomagnetic results confirm that the relative clockwise (CW) rotation of Eastern Liaoning-Korea Block (ELKB) with respect to NCB does not affect the Jiaodong Peninsula as a rigid block, nevertheless, some tectonic structures have been reactivated since Cenozoic and local rotations could be produced. This palaeomagnetic study reveals that the Late Mesozoic extension in Eastern Asia is heterogeneously expressed in time and space. The complete understanding of the mechanism(s) of this extensional event needs further multidisciplinary investigations.
ISSN: 0031-9201

insu-00599546
https://hal-insu.archives-ouvertes.fr/insu-00599546
https://hal-insu.archives-ouvertes.fr/insu-00599546/document
https://hal-insu.archives-ouvertes.fr/insu-00599546/file/Charles_et_al_PEPI2011.pdf
DOI : 10.1016/j.pepi.2011.05.006

Éditeur(s) : HAL CCSD Oxford University Press (OUP)
Résumé : International audience
We present a new interpretation of anisotropy of magnetic susceptibility (AMS) fabrics in basaltic lava flows based on the detailed study of magnetic mineralogy and silicate crystallographic fabric of a Quaternary lava flow from the French Massif Central (La Palisse). We consider the model of AMS fabric imbrication between magnetic foliation and flow surface, as initially proposed for dykes. At the two sampling sites, the concordance between the flow direction deduced from the AMS foliation and that deduced from field observations indicates that the imbrication model could apply to the lava flows. However, the flow senses inferred fromAMSare systematically opposed between the two sampling sites suggesting permutations between K1 and K3 AMS axes, a configuration referred to as inverse fabric. Electron backscatter diffraction (EBSD) measurements show strong lattice-preferred orientations (LPO) for plagioclase, especially the (010) plagioclase plane, which tends to be parallel to the flow. Clinopyroxene LPO remains less marked than plagioclase LPO, whereas titanomagnetite does not display a significant LPO. Comparison between magnetic and crystallographic fabrics suggests that the AMS fabric of the lava flow results from the distribution of titanomagnetite grains, which is in turn controlled by the fabric of the silicate framework. Magnetic hysteresis parameters and anisotropy of remanent magnetization (ARM) measurements exclude a significant contribution from single-domain grains, often called upon to explain inverse magnetic fabrics. The origin of the observed inverse magnetic fabric may relate to the dip of the palaeosurface, which is the only remarkable difference between the two sampling sites. AMS appears as a good tool to determine the direction of basaltic lava flows and coupling with local crystallographic fabric data provides a valuable control of relationships between magnetic fabrics and flow and thus contributes to better constrain the AMS signature of lava flows.
ISSN: 0956-540X

hal-00903561
https://hal.archives-ouvertes.fr/hal-00903561
https://hal.archives-ouvertes.fr/hal-00903561/document
https://hal.archives-ouvertes.fr/hal-00903561/file/TB-GJI-193-2-Orig.pdf
DOI : 10.1093/gji/ggs115

Éditeur(s) : HAL CCSD American Geophysical Union (AGU)
Résumé : International audience
The Tian Shan Mountains constitute central Asia's longest and highest mountain range. Understanding their Cenozoic uplift history thus bears on mountain building processes in general, and on how deformation has occurred under the influence of the India-Asia collision in particular. In order to help decipher the uplift history of the Tian Shan, we collected 970 samples for magnetostratigraphic analysis along a 4571-m-thick section at the Jingou River (Xinjiang Province, China). Stepwise alternating field and thermal demagnetization isolate a linear magnetization component that is interpreted as primary. From this component, a magnetostratigraphic column composed of 67 polarity chrons are correlated with the reference geomagnetic polarity timescale between ~1 Ma and ~23.6 Ma, with some uncertainty below ~21 Ma. This correlation places precise temporal control on the Neogene stratigraphy of the southern Junggar Basin and provides evidence for two significant stepwise increases in sediment accumulation rate at ~16–15 Ma and ~11–10 Ma. Rock magnetic parameters also undergo important changes at ~16–15 Ma and ~11–10 Ma that correlate with changes in sedimentary depositional environments. Together with previous work, we conclude that growth history of the modern Tian Shan Mountains includes two pulses of uplift and erosion at ~16–15 Ma and ~11–10 Ma. Middle to upper Tertiary rocks around the Tian Shan record very young (<~5 Ma) counterclockwise paleomagnetic rotations, on the order of 15° to 20°, which are interpreted as because of strain partitioning with a component of sinistral shear that localized rotations in the piedmont.
ISSN: 0278-7407

insu-00376345
https://hal-insu.archives-ouvertes.fr/insu-00376345
https://hal-insu.archives-ouvertes.fr/insu-00376345/document
https://hal-insu.archives-ouvertes.fr/insu-00376345/file/2007TC002137.pdf
DOI : 10.1029/2007TC002137

Éditeur(s) : HAL CCSD Springer/Terra Scientific Publishing Company
Résumé : International audience
We carried out a detailed paleomagnetic, rock-magnetic, and Thellier paleointensity study of all similar to 3.6 My Pliocene lava flow succession in southern Georgia. An earlier study (Camps et al., 1996) revealed that several consecutive lava flows record an intermediate polarity direction at the base of the section followed by a thick reverse polarity zone. The transitional field was interpreted as an excursion within chron 2Ar or all upper Cochiti-Gilbert reversal. New paleomagnetic data reported here have been obtained from nearby lava successions. In total, about 170 standard paleomagnetic cores belonging to 22 lava flows were collected during the 2005 sample collection campaign. Rock-magnetic experiments showed that the remanence is carried by Ti-poor titanomagnetite in most of the samples. The fraction of grains with multidomain magnetic structure does not seem to be important. Characteristic remanent magnetization was successfully determined oil all samples. The direct correlation with the original (Thoki) sequence, previous preliminary measurements of natural remanent magnetization (Sologashvili, 1986), and field observations allowed us to establish a new magnetic stratigraphy. The lower part of section is characterized by intermediate magnetic polarity followed by thick reversely magnetized lavas. The upper sequence, represented by 18 consecutive flows yielded normal magnetic polarity. The mean paleointensity of the intermediate field is drastically reduced with respect to the post-transitional field strength. Based on all available radiometric ages and new paleomagnetic data, it may be speculated that Gilbert-Gauss (R-N) reversal was recorded at the upper part of sequence. Lower intermediate polarity flows possibly represent a form of precursor of this reversal that is similar to the Matuyama-Brunhes geomagnetic transition.
ISSN: 1343-8832

hal-00413099
https://hal.archives-ouvertes.fr/hal-00413099

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
The Espinho Branco anatexite, located within a transcurrent, high-temperature shear zone in NE Brazil, was the subject of a comprehensive petrostructural study (Anisotropy of Magnetic Susceptibility - AMS, Anisotropy of Anhysteretic Remanence - AAR, Electron Backscatter Diffraction - EBSD) to evaluate the compatibility of different fabrics with the kinematics of melt deformation. Magnetite dominates susceptibilities larger than 1 mSI and biotite displays [001] lattice directions consistent with AMS k3 axes. In contrast, migmatites with a susceptibility lower than 0.5 mSI and no visible mesoscopic foliation provide crystallographic fabrics distinct from AMS and AAR. However, AAR remains consistent with the regional strain field. These results suggest that the correlation of field, AMS and crystallographic fabrics is not always straightforward despite the relatively simple organisation of the magnetic fabric in the anatexite. We conclude that AMS recorded the final stages of the strain field in the migmatite irrespective of its complex mesoscale structures and contrasting crystallographic fabrics.
ISSN: 0191-8141

hal-00823056
https://hal.archives-ouvertes.fr/hal-00823056
DOI : 10.1016/j.jsg.2012.12.008

Éditeur(s) : HAL CCSD Oxford University Press (OUP)
Résumé : International audience
Three kilns and a collection of baked bricks from Italian archaeological sites have been studied for archaeointensity determination using the Thellier method as modified by Coe. All sites are dated based on archaeological information and their ages range from 500 to 800 AD and 1500 to 1700 AD. Rock magnetic studies identify magnetite, Ti- magnetite and hematite as the main magnetic minerals, and magnetic susceptibility versus temperature shows a good thermal stability of the samples. The intensity results have been corrected for anisotropy of the thermoremanent magnetization and cooling rate effects. The new data together with 136 previously published results are used to estimate the variation of the Earth's magnetic field over the past three millennia. The time distribution of the Italian absolute intensity data is irregular with the majority of determinations concentrated during the last four centuries, while older periods are very poorly covered. Most of the data come from volcanic rocks and show significant discrepancies. All data have been compared with archaeointensity results from Europe and regional and global models predictions. This work indicates the need to obtain more high quality archaeointensity results, in particular for the periods older than 200 BC and between 200 and 1000 AD, in order to determine a robust Italian intensity secular variation curve that, in combination with directional data, could be used for archaeomagnetic dating.
ISSN: 0956-540X

hal-00452451
https://hal.archives-ouvertes.fr/hal-00452451
DOI : 10.1111/j.1365-246X.2009.04455.x

Éditeur(s) : HAL CCSD Elsevier
Résumé : Reliable measurements of the intensity of the palaeomagnetic field are notoriously difficult to obtain. The approach generally taken is to produce multiple estimates per rock unit and assume that those which meet certain minimum standards of technical quality will combine to produce an accurate mean. However, here, using results produced from a package of 20th century basaltic lava flows from Mount Etna in Sicily, we demonstrate that this approach can fail. In this case, the application of typical sets of selection criteria actually introduces bias into the mean determination that we measure. We demonstrate that this is caused by two types of non-ideal behaviour acting in combination. The first is a result of the multidomain grains that the samples contain and the second is caused by differences in the natural and laboratory cooling rates. We discuss means of avoiding these sources of error in future palaeointensity studies performed on ancient rocks. We also develop a new, more general reliability criterion which is effective here and which we argue should be applied wherever possible in future palaeointensity studies in conjunction with standard criteria. It requires two distinct types of materials which both produce some good-quality palaeointensity measurements and uses their range of overlap to constrain the true palaeointensity. Both the application of this criterion and general reliability considerations require that future palaeointensity studies should measure many samples per cooling unit and that these should be as diverse in terms of their rock magnetic properties and cooling histories as possible.
ISSN: 0012-821X

hal-00407943
https://hal.archives-ouvertes.fr/hal-00407943
DOI : 10.1016/j.epsl.2007.03.017

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
In the Arokam Tenere, the three studied massifs of granitoids are located around the N-S oriented Raghane mega-shear zone, which separates two of the main domains of the Tuareg shield, the Saharan metacraton and the Central Hoggar. The field observations, AMS analyses and U-Pb zircon dating were completed by a study of Landsat images because of the scarcity of outcrops in several parts of the studied area.;The image analysis allows to distinguish Arokam-East and Abdou granitoids in the eastern plutonic complex. It has also shown that the western plutonic complex corresponds to two different intrusions: the Yvonne granite and granodiorite. This is confirmed by the magnetic fabric that presents different characteristics in the different granitoids. U-Pb zircon dating and field observations show that the Arokam-West basement granite is much older (1915 Ma) than the Hanane granodiorite (582 Ma) in the central plutonic complex. Arokam-East and -West granites then belong to the Eburnean basement. The magnetic fabric of these granites is mainly associated with a post-magmatic deformation, probably of Pan-African age. Yvonne granodiorite is likely contemporaneous of the main displacement along the Raghane shear zone. The Yvonne granite (594 Ma) and Hanane granodiorite have a fabric similar to that previously obtained in most plutons of the Tiririne area. This fabric is related to the regional stress field, associated with the activity of the Raghane shear zone, during the late-magmatic phase in the plutons. On the contrary, the magnetic fabric of the Abdou pluton is still reflecting only the magma flow.
ISSN: 0899-5362

hal-00617478
https://hal.archives-ouvertes.fr/hal-00617478
DOI : 10.1016/j.jafrearsci.2011.02.007

Éditeur(s) : HAL CCSD Oxford University Press (OUP)
Résumé : International audience
IODP Expedition 352 cored igneous rocks from the Izu-Bonin-Mariana forearc crust. Cores from Sites U1440 and U1441 recovered Eocene basalts and related rocks and cores from Sites U1439 and U1442 recovered Eocene boninites and related rocks. We selected samples from Holes U1439C, U1440B and U1442A for palaeointensity measurements. Hysteresis measurements and high and low-temperature magnetization curves show that samples from Hole U1440B undergo magneto-chemical changes when heated and are mostly composed of single-domain (SD) or pseudo-single-domain (PSD) titanomaghemite. In contrast, the same measurements show that most selected samples from Holes U1439C and U1442A are thermally stable and are composed of either SD or PSD titanomagnetite with very little titanium content, or SD ferromagnetic grains with a large paramagnetic contribution. Thellier–Thellier palaeointensity experiments carried out on U1439C and U1442A samples give a good success rate of 25/60 and Virtual Dipole Moment (VDM) values between 1.3 and 3.5 × 1022 Am2. Multispecimen palaeointensity experiments with the domain-state corrected method carried out on 55 samples from Hole U1440B (divided into four groups) and 20 from Hole U1439C gave poor quality results, but indicated a VDM around 4–6 × 1022 Am2 in Hole U1440B forearc basalts. These results are in agreement with the few, low VDM values previously measured on Eocene rocks. However, they do not support an inverse relationship between field intensity and reversal rate for this period of time, since the Eocene reversal rate was low.
ISSN: 0956-540X

hal-01622775
https://hal.archives-ouvertes.fr/hal-01622775
https://hal.archives-ouvertes.fr/hal-01622775/document
https://hal.archives-ouvertes.fr/hal-01622775/file/carvalloGJI2017.pdf
DOI : 10.1093/gji/ggx208

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
Studies of paleomagnetic fields during polarity transitions recorded over the past few million years frequently suggest a configurational persistence consistent with long-lived mantle control over the pattern of flux emanating from Earth's fluid core. Fundamental to an understanding of the core-mantle dynamics involved is the question of the spatial-temporal nature of the physical conditions at the base of the mantle that may be responsible. Our analysis of the field during a mid-Cenozoic, reverse-to-normal (R-N) polarity change, recorded in a continuous sequence of lava flows in southeastern Queensland, Australia, provides strong evidence that the time span over which local mantle features retain such an influence is far longer than had thus far been observed. Specifically. the reversal is dominated by two sequential groupings of transitional magnetic vector directions, each associated with a clustering of virtual geomagnetic poles (VGPs) at locations common to several more youthful reversal datasets from about the globe. Our Ar-40/Ar-39 age determinations indicate that these Australian lavas erupted 25.56 +/- 0.48 Ma, strongly suggesting that the characteristic time for invariant control by the mantle over flux emerging from the outer core is at least on order of a few tens of Myr. The availability of transitional paleomagnetic data from still earlier times within the Cenozoic may further delineate this duration and, perhaps, provide a means to track changes in the pattern of long-standing concentrations of magnetic flux at the core-mantle boundary. (C) 2008 Elsevier B.V. All rights reserved.
ISSN: 0031-9201

hal-00411919
https://hal.archives-ouvertes.fr/hal-00411919
DOI : 10.1016/j.pepi.2008.07.012

Éditeur(s) : HAL CCSD Elsevier
Résumé : International audience
The easternmost part of the Neoproterozoic Araçuaí belt comprises an anatectic domain that involves anatexites (the Carlos Chagas unit), leucogranites and migmatitic granulites that display a well-developed fabric. Microstructural observations support that the deformation occurred in the magmatic to submagmatic state. Structural mapping integrating field and anisotropy of magnetic susceptibility (AMS) revealed a complex, 3D structure. The northern domain displays gently dipping foliations bearing a NW-trending lineation, southward, the lineation trend progressively rotates to EW then SW and the foliation is gently folded. The eastern domain displays E-W and NE-SW trending foliations with moderate to steeply dips bearing a dominantly NS trending lineation. Magnetic mineralogy investigation suggests biotite as the main carrier of the magnetic susceptibility in the anatexites and ferromagnetic minerals in the granulites. Crystallographic preferred orientation (CPO) measurements using the electron backscatter diffraction (EBSD) technique suggest that the magnetic fabric comes from the crystalline anisotropy of biotite and feldspar grains, especially. The delineation of several structural domains with contrasted flow fabric suggests a 3D flow field involving westward thrusting orthogonal to the belt, northwestward orogen-oblique escape tectonics and NS orogen-parallel flow. This complex deformation pattern may be due to interplay of collision-driven and gravity-driven deformations.
ISSN: 0191-8141

hal-00903878
https://hal.archives-ouvertes.fr/hal-00903878
DOI : 10.1016/j.jsg.2013.08.001

Éditeur(s) : HAL CCSD Springer/Terra Scientific Publishing Company
Résumé : International audience
Numerous phases of igneous activity took place in Egypt during the Mesozoic and the Cenozoic but no paleointensity results have ever been published from these rocks. Therefore a preliminary Survey was conducted in the northern part of Egypt and in Sinai to test the Suitability of these basalts for paleointensity determinations. Three Oligo-Miocene sites have been sampled north of Cairo: Abu Zaabal, Qatrani, and 6th of October City. In Sinai, we sampled Jurassic basalts in Wadi Budra and Oligo-Miocene rocks from Wadi Nukhul. The main magnetic carriers of these rocks are titanomagnetites with varying Ti content. Large secondary components are present in most middle Jurassic basalts and discrepancies remain in the directional analysis so this sill cannot be used for paleointensity experiments and the associated poles should not be considered for paleomagnetic reconstructions either. Directional analysis of the Oligo-Miocene basalts is very straightforward and updated mean VGPs have been calculated from the Cairo area (68.9 degrees N, 91.3 degrees E; Kappa = 274; A(95) = 3.7) and from Wadi Nukhul (72.7 degrees N, 13.4 degrees E; Kappa = 528; A(95) = 5.4). Pseudo-paleointensity results obtained as well from stable Egypt as from Sinai are promising, with values lower or similar (between 29 to 58 mu T) to present-day field intensity.
ISSN: 1343-8832

hal-00413086
https://hal.archives-ouvertes.fr/hal-00413086

Éditeur(s) : HAL CCSD Springer
Résumé : International audience
We present here a synthesis of the evolution of rifted continental margin systems in the Gulf of Aden. These margins are volcanic to the west of the Gulf of Aden, where they are influenced by the Afar hotspot, and non-volcanic east of longitude 46° E. The combined use of magnetics, gravity, seismic reflection, field observations (tectonic, stratigraphic and sedimentological) and oil well data allowed us to obtain better constraints on the timing of continental rifting and seafloor spreading. From the Permo-Triassic to the Oligocene, the Arabian-African plate was subject to distributed extension, probably due, at least from the Cretaceous, to tensile stresses related to the subduction of the Tethysian slab in the north. In Late Eocene-Early Oligocene, 34-33 Ma ago, rifting started to localise along the future area of continental breakup. Initially guided by the inherited basins, continental rifting then occurred synchronously over the entire gulf before becoming localised on the northern and southern borders of the inherited grabens, in the direction of the Afar hotspot. In the areas with non-volcanic margins (in the east), the faults marking the end of rifting trend parallel to the inherited grabens. Only the transfer faults cross-cut the inherited grabens, and some of these faults later developed into transform faults. The most important of these transform faults follow a Precambrian trend. Volcanic margins were formed in the west of the Gulf, up to the Guban graben in the southeast and as far as the southern boundary of the Bahlaf graben in the northeast. Seaward dipping reflectors can be observed on many oil industry seismic profiles. The influence of the hotspot during rifting was concentrated on the western part of the gulf. Therefore, it seems that the western domain was uplifted and eroded at the onset of rifting, while the eastern domain was characterised by more continuous sedimentation. The phase of distributed deformation was followed by a phase of strain localisation during the final rifting stage, just before formation of the Ocean-Continent Transition (OCT), in the most distal graben (DIM graben). About 20 Ma ago, at the time of the continental break-up, the emplacement of the OCT started in the east with exhumation of the subcontinental mantle. Farther west, the system was heated up by the strong influence of the Afar hotspot, which led to breakup with much less extension. In the Gulf of Aden (s.str), up to the Shukra El Sheik fracture zone, oceanic spreading started 17.6 Ma ago. West of this fracture zone, oceanic accretion started 10 Ma ago, and 2 Ma ago in the Gulf of Tadjoura. Post-rift deformation of the eastern margins of the Gulf of Aden can be seen in the distal and proximal domains. Indeed, the substantial post-rift uplift of these margins could be associated with either the continental break-up, or activity of the Afar hotspot and related volcanic/magmatic activity. Uplift of the northern proximal margin was still active (e.g. stepped beach rocks exposed at 60 m of 2 Ma; 30 m of 35,200 years; 10 and 2 m) and active volcanoes can be inferred at depths of between 70 and 200 km beneath the margin (at 5-10 km distance from the coast). On the distal margin, heat flow measurements show a high value that is associated with post-rift volcanic activity and the development of a volcano (with flows and sills) shortly after the formation of the OCT. The Afar hotspot is therefore important for several reasons. It allows the localisation of deformation along the Red Sea/Aden system and the rapid opening of the Gulf after the continental break-up; its influence also seems to persist during the post-rift period.
ISSN: 1866-7411

hal-01053089
https://hal.archives-ouvertes.fr/hal-01053089
DOI : 10.1007/s12517-011-0475-4